西部中医药
西部中醫藥
서부중의약
GANSU JOURNAL OF TRADITIONAL CHINESE MEDICINE
2014年
2期
34-35
,共2页
郭敏%王晓琳%黄聪琳%姜华
郭敏%王曉琳%黃聰琳%薑華
곽민%왕효림%황총림%강화
镰形棘豆%总黄酮%提取工艺
鐮形棘豆%總黃酮%提取工藝
렴형극두%총황동%제취공예
LianXing JiDou%total flavonoids%extraction process
目的:比较4种不同工艺对镰形棘豆总黄酮提取的影响。方法:采用水提醇沉酸解、水提、碱提酸沉及水提酸解4种工艺提取,以镰形棘豆总黄酮得率及纯度为指标,NaNO2-Al(NO3)3比色法测定镰形棘豆总黄酮含量。结果:镰形棘豆最佳提取工艺为水提酸解。该提取物中总黄酮提取率为1.6%,纯度为:11.26%。结论:该工艺可用于镰形棘豆药材中总黄酮成分的提取,方法可靠,简便易行。
目的:比較4種不同工藝對鐮形棘豆總黃酮提取的影響。方法:採用水提醇沉痠解、水提、堿提痠沉及水提痠解4種工藝提取,以鐮形棘豆總黃酮得率及純度為指標,NaNO2-Al(NO3)3比色法測定鐮形棘豆總黃酮含量。結果:鐮形棘豆最佳提取工藝為水提痠解。該提取物中總黃酮提取率為1.6%,純度為:11.26%。結論:該工藝可用于鐮形棘豆藥材中總黃酮成分的提取,方法可靠,簡便易行。
목적:비교4충불동공예대렴형극두총황동제취적영향。방법:채용수제순침산해、수제、감제산침급수제산해4충공예제취,이렴형극두총황동득솔급순도위지표,NaNO2-Al(NO3)3비색법측정렴형극두총황동함량。결과:렴형극두최가제취공예위수제산해。해제취물중총황동제취솔위1.6%,순도위:11.26%。결론:해공예가용우렴형극두약재중총황동성분적제취,방법가고,간편역행。
Objective:To compare the effects of four kinds of processes on the extraction of total flavonoids from LianXing JiDou(Oxytropis falcata Bunge). Methods:The contents of total flavonoids from LianXing JiDou were detected by NaNO2-Al(NO3) 3 chromatometry, the yield and the purity of total flavonoids were taken as the indexes, total flavonoids were extracted with the processes including water-extraction alcohol-precipitation and acid-hydroly-sis, water-extraction, alkaline-extraction and acid-precipitation, water-extraction and acid-hydrolysis. Results: The best extraction process for LianXing JiDou was water-extraction and acid-hydrolysis. The extraction percentage and the purity of total flavonoids were 1.6%and 11.26%respectively. Conclusion:The process could be used to extract total flavonoids from LianXing JiDou, which is reliable, simple and practicable.