化学研究与应用
化學研究與應用
화학연구여응용
CHEMICAL RESEARCH AND APPLICATION
2014年
1期
130-134
,共5页
雷宁%马萍%许本善%吕亚丽%杜树山%张以善
雷寧%馬萍%許本善%呂亞麗%杜樹山%張以善
뢰저%마평%허본선%려아려%두수산%장이선
甘肃蚤缀%脂溶性成分%气相色谱-质谱联用
甘肅蚤綴%脂溶性成分%氣相色譜-質譜聯用
감숙조철%지용성성분%기상색보-질보련용
Arenaria kansuensis Maxim.%liposoluble constituents%gas chromatography-mass spectrometry( GC-MS)
研究藏药甘肃蚤缀的脂溶性成分,进一步揭示该药材的化学成分,为这一传统藏药资源的开发利用提供实验依据。采用95%乙醇回流提取甘肃蚤缀全草,滤液浓缩后用石油醚萃取,得到脂溶性部位,通过气相色谱-质谱联用技术分析其化学成分,结合计算机检索技术及美国国家标准技术研究所( NIST)化合物谱库检索进行鉴定,采用面积归一化法确定其相对含量。从甘肃蚤缀石油醚部位共分离鉴定出25个化合物,相对含量占总含量的91.31%,包括脂肪类、甾体、三萜及芳香化合物等。
研究藏藥甘肅蚤綴的脂溶性成分,進一步揭示該藥材的化學成分,為這一傳統藏藥資源的開髮利用提供實驗依據。採用95%乙醇迴流提取甘肅蚤綴全草,濾液濃縮後用石油醚萃取,得到脂溶性部位,通過氣相色譜-質譜聯用技術分析其化學成分,結閤計算機檢索技術及美國國傢標準技術研究所( NIST)化閤物譜庫檢索進行鑒定,採用麵積歸一化法確定其相對含量。從甘肅蚤綴石油醚部位共分離鑒定齣25箇化閤物,相對含量佔總含量的91.31%,包括脂肪類、甾體、三萜及芳香化閤物等。
연구장약감숙조철적지용성성분,진일보게시해약재적화학성분,위저일전통장약자원적개발이용제공실험의거。채용95%을순회류제취감숙조철전초,려액농축후용석유미췌취,득도지용성부위,통과기상색보-질보련용기술분석기화학성분,결합계산궤검색기술급미국국가표준기술연구소( NIST)화합물보고검색진행감정,채용면적귀일화법학정기상대함량。종감숙조철석유미부위공분리감정출25개화합물,상대함량점총함량적91.31%,포괄지방류、치체、삼첩급방향화합물등。
The first study was to explore the chemical compounds of the liposoluble parts from Arenaria kansuensis Maxim,and pro-vide the test basis for further rational expoitation and utilization of its medicinal resources. The air-dried whole plants of Arenaria kansuensis Maxim. were extracted with 95% ethano1. The extract was concentrated and extracted with petroleum ether to get the li-posoluble parts,and the chemical composition was identified and analyzed by GC-MS method. Combining with computer retrieval technology and search of national institute of standards and technology( NIST) compound spectral-library for identification,their rela-tive content was determined by the area normalization method. Totally 25 compounds were identified and their corresponding relative contents were evaluated by area normalization method. The content of all identified compounds is 91. 31%,of them,most are ali-phatic derivatives,steroids,triterpene and aromatic compounds.