润滑与密封
潤滑與密封
윤활여밀봉
LUBRICATION ENGINEERING
2014年
2期
115-118
,共4页
电感耦合等离子体原子发射%润滑脂%灰化%酸解
電感耦閤等離子體原子髮射%潤滑脂%灰化%痠解
전감우합등리자체원자발사%윤활지%회화%산해
ICP-AES%grease%incineration%acidolysis
研究电感耦合等离子体原子发射（ICP-AES）测定润滑脂方法的前处理步骤，改进ASTMD7303中的润滑脂灰化酸解步骤及试剂，提出一种润滑脂元素光谱分析前处理方法。采用改进方法处理润滑脂得到的元素Fe、Ca、Zn、P、Mo、Li等的光谱数据与标准方法处理得到的数据一致，证明该方法可以作为监测润滑脂中元素含量的前处理方法。
研究電感耦閤等離子體原子髮射（ICP-AES）測定潤滑脂方法的前處理步驟，改進ASTMD7303中的潤滑脂灰化痠解步驟及試劑，提齣一種潤滑脂元素光譜分析前處理方法。採用改進方法處理潤滑脂得到的元素Fe、Ca、Zn、P、Mo、Li等的光譜數據與標準方法處理得到的數據一緻，證明該方法可以作為鑑測潤滑脂中元素含量的前處理方法。
연구전감우합등리자체원자발사（ICP-AES）측정윤활지방법적전처리보취，개진ASTMD7303중적윤활지회화산해보취급시제，제출일충윤활지원소광보분석전처리방법。채용개진방법처리윤활지득도적원소Fe、Ca、Zn、P、Mo、Li등적광보수거여표준방법처리득도적수거일치，증명해방법가이작위감측윤활지중원소함량적전처리방법。
The pretreatment procedures of testing lubricating greases by Inductively Coupled Plasma-Atomic Emission Spectrometry(ICP-AES)method were studied.By improving the procedures and analysis agents of lubricating grease incinera-tion and acidolysis in ASTMD7303 standard method,a pretreatment method of the lubricating grease element spectrum analy-sis was put forward.The spectrum analysis results of the elements of Fe,Ca,Zn,P,Mo and Li have good consistency for the two pretreatment methods of lubricating greases,the improved pretreatment method and the standard method,which proves that this improved method can be used as the pretreatment method of inspecting the elements content in lubricating greases.
