湖北工业大学学报
湖北工業大學學報
호북공업대학학보
JOURNAL OF HUBEI UNIVERSITY OF TECHNOLOGY
2014年
1期
108-110,120
,共4页
吴尧%万端极%吴正奇%廖宇杰%杨涛%马超
吳堯%萬耑極%吳正奇%廖宇傑%楊濤%馬超
오요%만단겁%오정기%료우걸%양도%마초
微波辅助提取%棉籽糖%微滤膜%纳滤膜
微波輔助提取%棉籽糖%微濾膜%納濾膜
미파보조제취%면자당%미려막%납려막
microwave-assisted extraction%raffinose%micro-filtration membrane%nano-filtration membrane
采用微波辅助技术从脱酚棉籽粕中提取棉籽糖,通过单因素和正交实验考察了微波处理时间、微波功率、料液比、pH 值对棉籽糖浸出率的影响,得出了棉籽糖最佳提取条件:微波处理时间9 min、微波功率650 W、料液比1∶10、pH 值2.5,在此条件下棉籽糖的浸出率为91.5%,经过微滤膜除杂和纳滤膜浓缩纯化后,棉籽糖纯度95%.最后,通过微滤膜和纳滤膜技术进一步纯化浓缩棉籽糖.
採用微波輔助技術從脫酚棉籽粕中提取棉籽糖,通過單因素和正交實驗攷察瞭微波處理時間、微波功率、料液比、pH 值對棉籽糖浸齣率的影響,得齣瞭棉籽糖最佳提取條件:微波處理時間9 min、微波功率650 W、料液比1∶10、pH 值2.5,在此條件下棉籽糖的浸齣率為91.5%,經過微濾膜除雜和納濾膜濃縮純化後,棉籽糖純度95%.最後,通過微濾膜和納濾膜技術進一步純化濃縮棉籽糖.
채용미파보조기술종탈분면자박중제취면자당,통과단인소화정교실험고찰료미파처리시간、미파공솔、료액비、pH 치대면자당침출솔적영향,득출료면자당최가제취조건:미파처리시간9 min、미파공솔650 W、료액비1∶10、pH 치2.5,재차조건하면자당적침출솔위91.5%,경과미려막제잡화납려막농축순화후,면자당순도95%.최후,통과미려막화납려막기술진일보순화농축면자당.
The microwave-assisted technology was employed to extract raffinose from cottonseed meal without gossypol.Effects of microwave time,microwave power ratio,material liquid ratio and pH value on extraction rate of raffinose by the single factor and orthogonal experiments were studied.The best ex-tract conditions of raffinose were obtained.Raffinose was purified by micro-filtration membrane and nano-filtration membrane technology.The results showed that the best extract conditions were:microwave time 9 min.,microwave power ratio 650W,material liquid ratio 1:10,pH=2.5.In these conditions,the extrac-tion rate of raffinose was 9 1 .5%.After purification by micro-filtration membrane purifying and nano-filtra-tion membrane enrichment,the purity of raffinose was 9 5%.