CAJ | 학술논문

GBW（ E）130398自2012年国家质量监督检验检疫总局批准后，在合成橡胶行业校准门尼粘度计、生产控制、人员考核、产品检验、产品贸易、质量仲裁等方面发挥了重要的作用，得到了广泛的应用。研制的该批门尼黏度国家标准物质GBW（ E）130398的量预计2013年年底将使用完，为满足合成橡胶行业对门尼黏度标准物质的需求，国家合成橡胶质量监督检验中心组织复制门尼黏度标准物质。经过样品候选、均匀性检验、稳定性检验、定值、不确定度评估等工作，GBW（E）130398标准物质被成功复制。门尼黏度标准物质定值结果在0.01的显著水平时，数据无异常值、呈现正态分布、各组数据间处于等精度。因此，定值结果的总平均值ML（1＋4）100℃（49.8±0.8）则为门尼黏度标准物质的标称值。
GBW（ E）130398자2012년국가질량감독검험검역총국비준후，재합성상효행업교준문니점도계、생산공제、인원고핵、산품검험、산품무역、질량중재등방면발휘료중요적작용，득도료엄범적응용。연제적해비문니점도국가표준물질GBW（ E）130398적량예계2013년년저장사용완，위만족합성상효행업대문니점도표준물질적수구，국가합성상효질량감독검험중심조직복제문니점도표준물질。경과양품후선、균균성검험、은정성검험、정치、불학정도평고등공작，GBW（E）130398표준물질피성공복제。문니점도표준물질정치결과재0.01적현저수평시，수거무이상치、정현정태분포、각조수거간처우등정도。인차，정치결과적총평균치ML（1＋4）100℃（49.8±0.8）칙위문니점도표준물질적표칭치。
GBW( E)130398 played important roles in the synthetic rubber industry calibration Mooney viscome-ter,production control,staff assessment,product inspecting,product trade,arbitration quality,and had been widely applied ,since 2012 ,the State Administration of Quality Supervision Inspection and Quarantine had been ratified.It was expected to at the end of 2013 would(will) be used up GBW(E)130398,in order to meet demand in rubber industry Mooney viscometer certified reference material ,the National Quality Supervision and Inspection Center of Synthetic Rubber organized to replicate Mooney viscosity standard substance.GBW ( E) 130398 standard substance had been successfully reproduced ,through selected the candidate sample ,tested sample's homogeneity and stability , setted value and evaluated uncertainty ,etc.When the significant level of fixed value was 0.01 ,the data were no du-bious value ,normal distribution and in equal precision.Therefore , the average ML ( 1 +4 ) 100℃( 49.8 ±0.8 ) of certification of Mooney viscosity certified reference material was normal value.