当代化工
噹代化工
당대화공
CONTEMPORARY CHEMICAL INDUSTRY
2014年
1期
76-79
,共4页
王亚平%解海龙%李石林%董登峰%侯海云
王亞平%解海龍%李石林%董登峰%侯海雲
왕아평%해해룡%리석림%동등봉%후해운
体积含水率%比重瓶%称量法
體積含水率%比重瓶%稱量法
체적함수솔%비중병%칭량법
Volumetric water content%Pycnometer%Weighing method
原油或油品含水率的精确测量对原油的生产开采、计量、储存和使用十分重要,目前有多种测量的方法和仪器,在使用中各有特点。导出了密度和含水率的关系原理,采用实验室常用的比重瓶和天平为测量装置,通过对空比重瓶、装满待测油样后的比重瓶的质量测定,即可得出待测油样的体积含水率。对两种油品的实验数据显示:油样中含水率在1%~99%间,含水率测量值和真实值在0.5%内一致。而且,含水率大、小,水、油乳化和分层对测量精度没有影响。并分析了实际误差大于方法误差的原因。
原油或油品含水率的精確測量對原油的生產開採、計量、儲存和使用十分重要,目前有多種測量的方法和儀器,在使用中各有特點。導齣瞭密度和含水率的關繫原理,採用實驗室常用的比重瓶和天平為測量裝置,通過對空比重瓶、裝滿待測油樣後的比重瓶的質量測定,即可得齣待測油樣的體積含水率。對兩種油品的實驗數據顯示:油樣中含水率在1%~99%間,含水率測量值和真實值在0.5%內一緻。而且,含水率大、小,水、油乳化和分層對測量精度沒有影響。併分析瞭實際誤差大于方法誤差的原因。
원유혹유품함수솔적정학측량대원유적생산개채、계량、저존화사용십분중요,목전유다충측량적방법화의기,재사용중각유특점。도출료밀도화함수솔적관계원리,채용실험실상용적비중병화천평위측량장치,통과대공비중병、장만대측유양후적비중병적질량측정,즉가득출대측유양적체적함수솔。대량충유품적실험수거현시:유양중함수솔재1%~99%간,함수솔측량치화진실치재0.5%내일치。이차,함수솔대、소,수、유유화화분층대측량정도몰유영향。병분석료실제오차대우방법오차적원인。
Accurate measurement of water content in crude oil an d oil product is very important in oil production, measurement, storage and usage. There are so many methods and instruments for measuring water content, in which, every method and instrument has its own characteristic. In this paper, the relation between the water content and density of the oil sample was derived and used as measurement principle;common inexpensive pycnometer and the balance were used to measure the water content of oil sample. The mass of the pycnometer full filled with oil sample was determined by the balance. Then the water content can be calculated by the derived equation. The experimental data show that the measurement errors are almost within 0.5% for the oil samples with water content of 1%~99%. Furthermore, the precision of measurement is not affected by water content, emulsification and phasesplitting between water and oil. Finally,the methodic error and experimental error were discussed.