CAJ | 학술논문

依据JJF1059.1-2012《测量不确定度评定与表示》，分析高效液相色谱法测定罗非鱼中孔雀石绿残留量不确定度的来源，从影响不确定度的标准溶液配制us、样品前处理up和仪器测量u 仪等3个主要因素，对不确定度各个分量进行计算和合成，得出罗非鱼中孔雀石绿的扩展不确定度U=0.88（k=2）。
의거JJF1059.1-2012《측량불학정도평정여표시》，분석고효액상색보법측정라비어중공작석록잔류량불학정도적래원，종영향불학정도적표준용액배제us、양품전처리up화의기측량u 의등3개주요인소，대불학정도각개분량진행계산화합성，득출라비어중공작석록적확전불학정도U=0.88（k=2）。
According to Measurement Uncertainty and Results Indication (JJF1059.1-2012), the sources of uncertainty in determination of malachite green residue in Oreochromis sp. by the method of HPLC were analyzed. And three factors of uncertainty, i.e. Malachite green (MG) standard solution, sample treatment and instrument measurement, were found out. Meanwhile, the uncertainty of each variable was evaluated and synthesized as well, and the result showed that the expanded uncertainty was 0.88 μg/kg (k=2).