CAJ | 학술논문

目的：对多金属氧酸盐α2-K8 P2 W17 NiO61的形貌和结构进行研究。方法运用高压静电纺丝和程序焙烧的方法，制备α2-K8P2W17NiO61纳米粒子。结果红外光谱（FT-IR），X-射线粉末衍射数据（XRD）表明制备的纳米材料依然保持了Dawson-Wells结构，扫描电子显微镜（ SEM ）和半径分布图显示焙烧后得到的α2-K8 P2 W17 NiO61纳米纤维直径约为168 nm。结论成功获得了具有纳米纤维形貌的多金属氧酸盐：α2-K8 P2 W17 NiO61。
목적：대다금속양산염α2-K8 P2 W17 NiO61적형모화결구진행연구。방법운용고압정전방사화정서배소적방법，제비α2-K8P2W17NiO61납미입자。결과홍외광보（FT-IR），X-사선분말연사수거（XRD）표명제비적납미재료의연보지료Dawson-Wells결구，소묘전자현미경（ SEM ）화반경분포도현시배소후득도적α2-K8 P2 W17 NiO61납미섬유직경약위168 nm。결론성공획득료구유납미섬유형모적다금속양산염：α2-K8 P2 W17 NiO61。
Objective To Study the morphology and structure of polyoxometalates α2-K8 P2 W17 NiO61 .Methods Theα2-K8 P2 W17 NiO61 nanofibers were obtained through electrospinning technology and calcinations method .Results The datas of Fourier transformation infrared spectroscopy and X-ray diffraction showed that the Dawson-Wells struc-ture of the polyoxometalates was still remained in the fibrous membranes .Scanning electron microscopy images and di-ameter distribution curves of the fibrous membranes indicated that the average diameter of α2-K8 P2 W17 NiO61 was about 168 nm.Conclusion The nanofibers of polyoxometalates α2-K8 P2 W17 NiO61 were successfully prepared .