西北药学杂志
西北藥學雜誌
서북약학잡지
2014年
2期
111-114
,共4页
胡曙晨%马雪红%李新霞%李莉%热娜·卡斯木%支玲
鬍曙晨%馬雪紅%李新霞%李莉%熱娜·卡斯木%支玲
호서신%마설홍%리신하%리리%열나·잡사목%지령
肉桂%桂皮醛%β-谷甾醇%薄层鉴别
肉桂%桂皮醛%β-穀甾醇%薄層鑒彆
육계%계피철%β-곡치순%박층감별
Cinnamomum cassia Presl%cinnamic aldehyde%β-sitosterol%TLC identification
目的:建立肉桂子药材的薄层鉴别系统。方法以桂皮醛和β-谷甾醇为对照品,对维药肉桂子进行薄层鉴别,并考察不同展开系统、不同点样量、不同薄层板、不同检视方式、不同温度和不同湿度对肉桂子药材薄层色谱的影响。结果以桂皮醛和β-谷甾醇为对照品,正己烷-乙酸乙酯(6∶1)为展开系统,肉桂子药材薄层鉴别特征明显,专属性强。结论该薄层方法可行,重复性好,可作为肉桂子药材的薄层鉴别方法。
目的:建立肉桂子藥材的薄層鑒彆繫統。方法以桂皮醛和β-穀甾醇為對照品,對維藥肉桂子進行薄層鑒彆,併攷察不同展開繫統、不同點樣量、不同薄層闆、不同檢視方式、不同溫度和不同濕度對肉桂子藥材薄層色譜的影響。結果以桂皮醛和β-穀甾醇為對照品,正己烷-乙痠乙酯(6∶1)為展開繫統,肉桂子藥材薄層鑒彆特徵明顯,專屬性彊。結論該薄層方法可行,重複性好,可作為肉桂子藥材的薄層鑒彆方法。
목적:건립육계자약재적박층감별계통。방법이계피철화β-곡치순위대조품,대유약육계자진행박층감별,병고찰불동전개계통、불동점양량、불동박층판、불동검시방식、불동온도화불동습도대육계자약재박층색보적영향。결과이계피철화β-곡치순위대조품,정기완-을산을지(6∶1)위전개계통,육계자약재박층감별특정명현,전속성강。결론해박층방법가행,중복성호,가작위육계자약재적박층감별방법。
Objective To establish a thin-layer chromatography(TLC) identification method for the Uygur medicine Fructus cinnam-omi cassiae immaturi .Methods With cinnamic aldehyde and β-sitosterol as the references substances ,the TLC conditions ,such as the development system ,spotting sample volume ,thin layer chromatography plate ,inspection ,temperature and humidity ,were investigated .Results With cinnamic aldehyde andβ-sitosterol as the reference substances ,TLC identification for Fructus cinnam-omi cassiae immaturi was high specific with cyclohexane-ethyl acetate(6∶1) as the deployment system .Conclusion The estab-lished method is feasible and reproducible and could be used as the Fructus cinnamomi cassiae immaturi identification .