钛工业进展
鈦工業進展
태공업진전
TAI GONGYE JINZHAN
2014年
1期
42-45
,共4页
刘彩利%周军%石明华%李中奎
劉綵利%週軍%石明華%李中奎
류채리%주군%석명화%리중규
Zr-4合金%对比样%酸洗预处理%腐蚀增重
Zr-4閤金%對比樣%痠洗預處理%腐蝕增重
Zr-4합금%대비양%산세예처리%부식증중
Zr-4 alloy%contrast sample%acid washing pretreatment%steam corrosion weight gain
Zr-4合金和M5锆合金是国内核电站最常用的核反应堆包壳材料,其耐腐蚀性能是一项重要的检测指标。在高压釜蒸汽腐蚀实验中,为了确认腐蚀数据的有效性,每釜应随检测样品放置对比样。针对Zr-4合金作为对比样时的酸洗预处理工艺开展实验,研究是否酸洗及酸洗工艺对其腐蚀增重的影响,以期为建立Zr-4合金对比样规范提供科学的试验方法。研究结果表明,酸洗预处理会明显影响Zr-4合金的腐蚀增重及其标准偏差,未经酸洗处理的Zr-4合金对比样的腐蚀增重较稳定,标准偏差及增重极差值均低于经酸洗预处理的对比样。
Zr-4閤金和M5鋯閤金是國內覈電站最常用的覈反應堆包殼材料,其耐腐蝕性能是一項重要的檢測指標。在高壓釜蒸汽腐蝕實驗中,為瞭確認腐蝕數據的有效性,每釜應隨檢測樣品放置對比樣。針對Zr-4閤金作為對比樣時的痠洗預處理工藝開展實驗,研究是否痠洗及痠洗工藝對其腐蝕增重的影響,以期為建立Zr-4閤金對比樣規範提供科學的試驗方法。研究結果錶明,痠洗預處理會明顯影響Zr-4閤金的腐蝕增重及其標準偏差,未經痠洗處理的Zr-4閤金對比樣的腐蝕增重較穩定,標準偏差及增重極差值均低于經痠洗預處理的對比樣。
Zr-4합금화M5고합금시국내핵전참최상용적핵반응퇴포각재료,기내부식성능시일항중요적검측지표。재고압부증기부식실험중,위료학인부식수거적유효성,매부응수검측양품방치대비양。침대Zr-4합금작위대비양시적산세예처리공예개전실험,연구시부산세급산세공예대기부식증중적영향,이기위건립Zr-4합금대비양규범제공과학적시험방법。연구결과표명,산세예처리회명현영향Zr-4합금적부식증중급기표준편차,미경산세처리적Zr-4합금대비양적부식증중교은정,표준편차급증중겁차치균저우경산세예처리적대비양。
Zr-4 alloy and M5 zirconium alloy are the most useful cladding materials in nuclear power reactor .It is an important testing index for their corrosion resistance .In order to confirm the validity of corrosion weight gain data , it must be put contrast samples in autoclave at the experiment of steam corrosion .In this paper , acid washing pretreat-ment technologies for Zr-4 alloy were done , and the influence of acid washing pretreatment on steam corrosion weight gain was tested .It would be a scientific method for establishing Zr-4 alloy standard as contrast samples .The results show that the acid washing process has significant effect on weight gain and standard deviations of Zr -4 alloy.Samples which unwashed have stable weight gain and the standard deviation are less than the acid -washed samples .