中国有色金属学报
中國有色金屬學報
중국유색금속학보
THE CHINESE JOURNAL OF NONFERROUS METALS
2014年
2期
380-386
,共7页
Al-Mn合金%均匀化%性能%显微组织%析出相
Al-Mn閤金%均勻化%性能%顯微組織%析齣相
Al-Mn합금%균균화%성능%현미조직%석출상
Al-Mn alloy%homogenization%property%microstructure%precipitated phase
通过差热分析、金相显微镜、扫描电子显微镜、能谱分析、硬度和电导率测试等方法,对一种新型Al-Mn合金铸锭均匀化过程中的组织演变和性能变化规律进行研究。结果表明:在加热温度为560~620℃、保温时间为12~72 h的均匀化处理过程中,合金铸锭的电导率随温度的升高或保温时间的延长逐渐降低,但硬度先持续降低后在高于600℃均匀化时反而升高;合金铸锭由枝晶和晶间非平衡相组成,随均匀化温度的升高和保温时间的延长,晶间析出相逐渐溶解、球化,晶内细小弥散相大量析出;合金较优的热处理制度为600℃、24 h。
通過差熱分析、金相顯微鏡、掃描電子顯微鏡、能譜分析、硬度和電導率測試等方法,對一種新型Al-Mn閤金鑄錠均勻化過程中的組織縯變和性能變化規律進行研究。結果錶明:在加熱溫度為560~620℃、保溫時間為12~72 h的均勻化處理過程中,閤金鑄錠的電導率隨溫度的升高或保溫時間的延長逐漸降低,但硬度先持續降低後在高于600℃均勻化時反而升高;閤金鑄錠由枝晶和晶間非平衡相組成,隨均勻化溫度的升高和保溫時間的延長,晶間析齣相逐漸溶解、毬化,晶內細小瀰散相大量析齣;閤金較優的熱處理製度為600℃、24 h。
통과차열분석、금상현미경、소묘전자현미경、능보분석、경도화전도솔측시등방법,대일충신형Al-Mn합금주정균균화과정중적조직연변화성능변화규률진행연구。결과표명:재가열온도위560~620℃、보온시간위12~72 h적균균화처리과정중,합금주정적전도솔수온도적승고혹보온시간적연장축점강저,단경도선지속강저후재고우600℃균균화시반이승고;합금주정유지정화정간비평형상조성,수균균화온도적승고화보온시간적연장,정간석출상축점용해、구화,정내세소미산상대량석출;합금교우적열처리제도위600℃、24 h。
The evolution of microstructure and properties of a new Al-Mn alloy ingot during homogenization treatment was researched by differential scanning calorimetry (DSC), optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), as well as measurement of hardness and conductivity test, respectively. The results show that both the conductivity and the hardness of Al-Mn alloy ingot decrease with the increase of temperature in the range of 560-620℃or the extension of holding time in the range of 12-72 h, but hardness at 620℃is higher than that at 600 ℃. The cast alloy is composed of dendrite segregation and non-equilibrium phase. The precipitated phases gradually dissolve and become spherical, and the dispersity of precipitates within the grains increases with increasing homogenization temperature and holding time. The reasonable homogenization condition for the studied alloy is 600℃and 24 h.