CAJ | 학술논문

选取n(SiO2)∶n(Al2O3)、n(Na2O)∶n(Al2O3)、n(H2O)∶n(Al2O3)摩尔比为因素设计正交实验，以高岭土为主要原料制备了偏高岭土基地聚合物。依据高岭土的TG-DSC曲线和地聚合物试样抗压强度确定高岭土最佳煅烧温度为800℃。根据正交实验抗压强度结果分析了各因素的影响规律，确定最佳配比为：n(SiO2)∶n(Al2O3)为4、n(Na2O)∶n(Al2O3)为0.8、n(H2O)∶n(Al2O3)为17。对试样进行XRD表征，结果表明，XRD在20。~40。出现非晶馒头峰，可见已合成一种“半晶态”物质。
선취n(SiO2)∶n(Al2O3)、n(Na2O)∶n(Al2O3)、n(H2O)∶n(Al2O3)마이비위인소설계정교실험，이고령토위주요원료제비료편고령토기지취합물。의거고령토적TG-DSC곡선화지취합물시양항압강도학정고령토최가단소온도위800℃。근거정교실험항압강도결과분석료각인소적영향규률，학정최가배비위：n(SiO2)∶n(Al2O3)위4、n(Na2O)∶n(Al2O3)위0.8、n(H2O)∶n(Al2O3)위17。대시양진행XRD표정，결과표명，XRD재20。~40。출현비정만두봉，가견이합성일충“반정태”물질。
The n(SiO2)∶n(Al2O3), n(Na2O)∶n(Al2O3) and n(H2O)∶n(Al2O3) molar ratios were investigated by orthogonal experiment. The metakaolin based geopolymer was synthesized by kaolin. The optimum calcination temperature of kaolin was 800℃based on the TG-DSC curve of kaolin and compressive strength of specimens. Based on compressive strength, the effects of the three molar ratios were analyzed, the optimum molar ratio was n(SiO2)∶n(Al2O3) being 4, n(Na2O)∶n(Al2O3) being 0.8, n(H2O)∶n(Al2O3) being 17. X-ray Diffraction (XRD) was used to characterize the sample, the XRD analysis results indicated that the amorphous hump of metakaolin appeared at 20°~40°, a semi crystalline material was synthesized.