环境监控与预警
環境鑑控與預警
배경감공여예경
ENVIRONMENTAL MONITORING AND FOREWARNING
2014年
2期
21-24
,共4页
液液萃取%气相色谱 -质谱法%酞酸酯%百菌清%联苯胺
液液萃取%氣相色譜 -質譜法%酞痠酯%百菌清%聯苯胺
액액췌취%기상색보 -질보법%태산지%백균청%련분알
Liquid-Liquid Extraction%GC-MS%Phthalate ester%Chlorothalonil%Benzidine
建立了液液萃取-气相色谱-质谱（LLE -GC/MS）同时测定饮用水中的6种酞酸酯类化合物、百菌清和联苯胺的方法。选用3种有机溶剂进行萃取，筛选出回收率高、操作简单的前处理方法，萃取后经气相色谱-质谱分析。方法表明：8种物质线性良好，相关系数为0．9978～0．9995，用二氯甲烷萃取回收率最佳，回收率在90．1％～118％之间，相对标准偏差在0．24％～7．21％之间。
建立瞭液液萃取-氣相色譜-質譜（LLE -GC/MS）同時測定飲用水中的6種酞痠酯類化閤物、百菌清和聯苯胺的方法。選用3種有機溶劑進行萃取，篩選齣迴收率高、操作簡單的前處理方法，萃取後經氣相色譜-質譜分析。方法錶明：8種物質線性良好，相關繫數為0．9978～0．9995，用二氯甲烷萃取迴收率最佳，迴收率在90．1％～118％之間，相對標準偏差在0．24％～7．21％之間。
건립료액액췌취-기상색보-질보（LLE -GC/MS）동시측정음용수중적6충태산지류화합물、백균청화련분알적방법。선용3충유궤용제진행췌취，사선출회수솔고、조작간단적전처리방법，췌취후경기상색보-질보분석。방법표명：8충물질선성량호，상관계수위0．9978～0．9995，용이록갑완췌취회수솔최가，회수솔재90．1％～118％지간，상대표준편차재0．24％～7．21％지간。
A method was developed for the determination of 6 phthalate ester,chlorothalonil and benzidine in drinking water using LLE-GC/MS.The sample was extracted by dichloromethane,n-hexane and cyclohexane,separately.A simple extraction method with high recoveries was chosen.Then the compounds were determined by GC-MS.The result indicated that the calibration curves showed good linear relationship.The correlation coefficients were in the range of 0.997 8 ~0.999 5.Samples extracted with dichlo-romethane showed the highest recovery.The recoveries of 8 compounds were in range of 90.1% ~1 1 8% and the relative standard deviations were 0.24% ~7.21%.The method was suitable for the determination of phthalate ester,chlorothalonil and benzidine in surface water.
