按摩与康复医学
按摩與康複醫學
안마여강복의학
Chinese Manipulation & Rehabilitation Medicine
2014年
3期
144-146,147
,共4页
活血止痛片%薄层色谱法%高效液相色谱法%芍药苷%质量标准
活血止痛片%薄層色譜法%高效液相色譜法%芍藥苷%質量標準
활혈지통편%박층색보법%고효액상색보법%작약감%질량표준
Huoxuezhitong tablet%TLC%HPLC%paeoniflorin%quality standard
目的：建立活血止痛片的质量控制方法。方法：采用薄层色谱法对活血止痛片中的赤芍、当归、三七进行鉴别；采用高效液相色谱法对活血止痛片中的芍药苷进行定量。结果：赤芍、当归、三七薄层色谱斑点清晰，阴性无干扰；芍药苷在51.52~1288.0ng的范围内呈良好的线性关系，r=0.99995，平均加样回收率为99.79%，RSD=1.21%。结论：该方法简便准确，重现性好，可作为活血止痛片的质量控制标准。
目的：建立活血止痛片的質量控製方法。方法：採用薄層色譜法對活血止痛片中的赤芍、噹歸、三七進行鑒彆；採用高效液相色譜法對活血止痛片中的芍藥苷進行定量。結果：赤芍、噹歸、三七薄層色譜斑點清晰，陰性無榦擾；芍藥苷在51.52~1288.0ng的範圍內呈良好的線性關繫，r=0.99995，平均加樣迴收率為99.79%，RSD=1.21%。結論：該方法簡便準確，重現性好，可作為活血止痛片的質量控製標準。
목적：건립활혈지통편적질량공제방법。방법：채용박층색보법대활혈지통편중적적작、당귀、삼칠진행감별；채용고효액상색보법대활혈지통편중적작약감진행정량。결과：적작、당귀、삼칠박층색보반점청석，음성무간우；작약감재51.52~1288.0ng적범위내정량호적선성관계，r=0.99995，평균가양회수솔위99.79%，RSD=1.21%。결론：해방법간편준학，중현성호，가작위활혈지통편적질량공제표준。
Objective:To establish the quality standards of Huoxuezhitong tablet. Methods:TLC was used to distinguish the Radix Paeoniae Rubra, Radix Angelicae sinensis and Radix Notoginseng in Huoxuezhitong tablet;The content of paeoniflorin was determined by HPLC. Results:The pre-scription of Radix Paeoniae Rubra, Radix Angelicae sinensis and Radix Notoginseng has distinguishing characteristics without the interference of the blank control. Paeoniflorin in the framework of 51.52-1288.0ng showed a good linear relationship, r=0.9999, the average recovery was 99.79%, RSD=1.21%. Conclusion:This method is simple, accurate and reproducible, it can be used to control the quality of Huoxuezhitong tablet.
