CAJ | 학술논문

目的：建立一种安息香荧光衍生法测定面粉及其制品中硼砂根的含量。方法安息香与硼离子形成复合物，在甘氨酸做缓冲溶液条件下，通过荧光分光光度法测定复合物中的硼，进而建立一种快速检测食品中的硼砂含量的方法。结果在该条件下硼砂根为10-7~10-5 mol/L范围内回归系数达到0.9999。利用该条件建立的测定面制品中硼砂的含量回收率为83%~102%，其中面粉中的回收率在100%左右。结论本研究证明使用该方法测定面粉及其制品中的硼酸根较为准确、可靠，为方便快速地测定食品中的硼砂提供了技术支持。
목적：건립일충안식향형광연생법측정면분급기제품중붕사근적함량。방법안식향여붕리자형성복합물，재감안산주완충용액조건하，통과형광분광광도법측정복합물중적붕，진이건립일충쾌속검측식품중적붕사함량적방법。결과재해조건하붕사근위10-7~10-5 mol/L범위내회귀계수체도0.9999。이용해조건건립적측정면제품중붕사적함량회수솔위83%~102%，기중면분중적회수솔재100%좌우。결론본연구증명사용해방법측정면분급기제품중적붕산근교위준학、가고，위방편쾌속지측정식품중적붕사제공료기술지지。
Objectvie To develop a benzoin fluorescence method for the determination of borax in flour and its products. Methods Benzoin and boron ions formed complexes in glycine buffer solution and then de-termined by fluorescence spectrophotometry, thereby establishing a method for rapid detection of food borax content. Results Under the described conditions, the proposed method was applicable over the concentration range ( 10-7~10-5 mol/L), the borate concentration was linear with the fluorescence intensity (regression coef-ficient: 0.9999), with recoveries for borax in flour and related products were almost 100and 83~102 respec-tively. Conclusion The established method for determination of borax in flour and its products is accurate and validated, which provides efficient technical support for rapidly detecting the borax in food.