食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2014年
4期
27-32
,共6页
杨春月%朱靖博%王振中%肖伟
楊春月%硃靖博%王振中%肖偉
양춘월%주정박%왕진중%초위
复合乳化剂%HLB值%薯蓣皂苷%水提取
複閤乳化劑%HLB值%藷蕷皂苷%水提取
복합유화제%HLB치%서여조감%수제취
composite emulsifiers%HLB value%dioscin%extract in water
以span-60和tween-40配制而成的不同HLB值复合乳化剂研究不同HLB值及不同复合乳化剂添加量对薯蓣皂苷在水中分布的影响。通过单因素试验考察了HLB值与薯蓣皂素在水提取物及水提取物上清液中含量的关系,并考察不同复合乳化剂添加量与薯蓣皂素在水提取物及水提取物上清液中含量的关系。结果显示HLB值在4~12范围内,HLB值为8的乳化剂对用水提取的薯蓣皂苷的增溶作用最强;HLB值在12~15.6范围内,HLB值为15.6的乳化剂对用水提取的薯蓣皂苷增溶作用最强;HLB值在4~15.6范围内,HLB值为15.6的乳化剂对用水提取的薯蓣皂苷增溶作用最强;HLB值在4~15.6范围内,乳化剂对水提取薯蓣皂苷离心后的上清液中皂苷浓度影响不大;HLB值为8和15.6的复合乳化剂添加量为1.5%时,对薯蓣皂苷在水提物及水提物上清中增溶效果最好。
以span-60和tween-40配製而成的不同HLB值複閤乳化劑研究不同HLB值及不同複閤乳化劑添加量對藷蕷皂苷在水中分佈的影響。通過單因素試驗攷察瞭HLB值與藷蕷皂素在水提取物及水提取物上清液中含量的關繫,併攷察不同複閤乳化劑添加量與藷蕷皂素在水提取物及水提取物上清液中含量的關繫。結果顯示HLB值在4~12範圍內,HLB值為8的乳化劑對用水提取的藷蕷皂苷的增溶作用最彊;HLB值在12~15.6範圍內,HLB值為15.6的乳化劑對用水提取的藷蕷皂苷增溶作用最彊;HLB值在4~15.6範圍內,HLB值為15.6的乳化劑對用水提取的藷蕷皂苷增溶作用最彊;HLB值在4~15.6範圍內,乳化劑對水提取藷蕷皂苷離心後的上清液中皂苷濃度影響不大;HLB值為8和15.6的複閤乳化劑添加量為1.5%時,對藷蕷皂苷在水提物及水提物上清中增溶效果最好。
이span-60화tween-40배제이성적불동HLB치복합유화제연구불동HLB치급불동복합유화제첨가량대서여조감재수중분포적영향。통과단인소시험고찰료HLB치여서여조소재수제취물급수제취물상청액중함량적관계,병고찰불동복합유화제첨가량여서여조소재수제취물급수제취물상청액중함량적관계。결과현시HLB치재4~12범위내,HLB치위8적유화제대용수제취적서여조감적증용작용최강;HLB치재12~15.6범위내,HLB치위15.6적유화제대용수제취적서여조감증용작용최강;HLB치재4~15.6범위내,HLB치위15.6적유화제대용수제취적서여조감증용작용최강;HLB치재4~15.6범위내,유화제대수제취서여조감리심후적상청액중조감농도영향불대;HLB치위8화15.6적복합유화제첨가량위1.5%시,대서여조감재수제물급수제물상청중증용효과최호。
Effect of different HLB value composite emulsifiers which was prepared by span-60 and tween-40 and emulsifier amount ondioscin distribution in waterwere investigated. The relationships between the HLB value and content of diosgenin in water extract and water extract supernatant, and between the different amount of emulsifiers and content of diosgenin in water extract and water extract supernatant were examinedthrough the single factor experiments. The results showed as follows:whenHLB value was in the 4 to 12 range, there was the strongestdioscinsolubilizationin water extraction for HLB value of 8 compositeemulsifier.WhenHLB value was in the 12-15.6 range, there was the strongestdioscinsolubilization in water extraction for HLB value of 15.6 composite emulsifier .When HLB value was in the 4-15.6 range, there was thesolubilization strongest dioscinin water extraction for HLB value of 15.6 composite emulsifier.WhenHLB value was in the 4-15.6 range, there was not obvious impact on dioscin concentration in the supernatant fluid after centrifugation of water extraction for composite emulsifier. Composite emulsifiers with HLB value of 8 and 15.6 that content was 1.5 % had the bestsolubilization effect on dioscin in the water extraction and supernatant of water extraction.