新乡学院学报
新鄉學院學報
신향학원학보
Journal of Xinxiang University
2014年
8期
20-23
,共4页
水热合成%ZnTe纳米材料%合成条件
水熱閤成%ZnTe納米材料%閤成條件
수열합성%ZnTe납미재료%합성조건
hydrothermal synthesis%ZnTe nanomaterials%synthesis condition
用Zn粉和Te粉为原材料,利用水热合成法在不同条件下合成出不同结构的ZnTe纳米材料。用X 射线衍射仪、扫描电子显微镜和透射电子显微镜对合成的ZnTe纳米材料进行了表征,研究了合成条件对纳米ZnTe结构的影响。结果表明,在无机NaOH溶液中易形成ZnTe纳米晶体颗粒,而在有机水合肼溶液中易形成非晶ZnTe纳米片或纳米线,非晶ZnTe纳米材料通过退火处理很容易地转化成晶体纳米材料。研究结果丰富了ZnTe纳米材料的合成知识,并为ZnTe纳米材料的应用研究奠定了基础。
用Zn粉和Te粉為原材料,利用水熱閤成法在不同條件下閤成齣不同結構的ZnTe納米材料。用X 射線衍射儀、掃描電子顯微鏡和透射電子顯微鏡對閤成的ZnTe納米材料進行瞭錶徵,研究瞭閤成條件對納米ZnTe結構的影響。結果錶明,在無機NaOH溶液中易形成ZnTe納米晶體顆粒,而在有機水閤肼溶液中易形成非晶ZnTe納米片或納米線,非晶ZnTe納米材料通過退火處理很容易地轉化成晶體納米材料。研究結果豐富瞭ZnTe納米材料的閤成知識,併為ZnTe納米材料的應用研究奠定瞭基礎。
용Zn분화Te분위원재료,이용수열합성법재불동조건하합성출불동결구적ZnTe납미재료。용X 사선연사의、소묘전자현미경화투사전자현미경대합성적ZnTe납미재료진행료표정,연구료합성조건대납미ZnTe결구적영향。결과표명,재무궤NaOH용액중역형성ZnTe납미정체과립,이재유궤수합정용액중역형성비정ZnTe납미편혹납미선,비정ZnTe납미재료통과퇴화처리흔용역지전화성정체납미재료。연구결과봉부료ZnTe납미재료적합성지식,병위ZnTe납미재료적응용연구전정료기출。
ZnTe nanomaterials with different structures were synthesized under different conditions by using hydro-thermal method ,where Zn and Te powders were used as the source materials .The nanomaterials were characterized by X-ray diffractometer ,scanning electron microscope and transmission electron microscope .The effects of synthe-sis conditions on ZnTe nanostructures were studied . Results indicated that ZnTe crystalline nanoparticles wre formed easily in inorganic NaOH solution ,while amorphous ZnTe nanosheets or nanowires were formed easily in or-ganic hydrazine solution which converted into crystalline structure by annealing .The research results enriched the knowledge about the synthesis of ZnTe nanomaterials and contributed to the application researches of ZnTe nanoma-terials .