化工时刊
化工時刊
화공시간
CHEMICAL INDUSTRY TIMES
2014年
8期
16-19,24
,共5页
杨郭%李玉芝%李莉%梁晓峰%冯长林
楊郭%李玉芝%李莉%樑曉峰%馮長林
양곽%리옥지%리리%량효봉%풍장림
贯叶连翘%金丝桃素%微波提取%二次回归通用旋转组合设计
貫葉連翹%金絲桃素%微波提取%二次迴歸通用鏇轉組閤設計
관협련교%금사도소%미파제취%이차회귀통용선전조합설계
Hypericum perforatum%Hypericin%microwave extraction%quadratic general rotary unitized design
通过微波提取方法研究贯叶连翘中金丝桃素的提取工艺。通过单因素实验研究了微波功率,液固比,乙醇浓度,微波温度以及微波时间对金丝桃素提取率的影响,通过二次回归通用旋转组合设计研究了微波功率,液固比,乙醇浓度,微波温度以及微波时间对提取率的影响。二次回归通用旋转组合设计的最优工艺条件是:17.5倍量的65%的乙醇溶液,在65℃下用700 W的微波提取64 min。通过微波提取方法较传统的浸提法具有耗时短,提取率高的特点,具有较好的应用前景。
通過微波提取方法研究貫葉連翹中金絲桃素的提取工藝。通過單因素實驗研究瞭微波功率,液固比,乙醇濃度,微波溫度以及微波時間對金絲桃素提取率的影響,通過二次迴歸通用鏇轉組閤設計研究瞭微波功率,液固比,乙醇濃度,微波溫度以及微波時間對提取率的影響。二次迴歸通用鏇轉組閤設計的最優工藝條件是:17.5倍量的65%的乙醇溶液,在65℃下用700 W的微波提取64 min。通過微波提取方法較傳統的浸提法具有耗時短,提取率高的特點,具有較好的應用前景。
통과미파제취방법연구관협련교중금사도소적제취공예。통과단인소실험연구료미파공솔,액고비,을순농도,미파온도이급미파시간대금사도소제취솔적영향,통과이차회귀통용선전조합설계연구료미파공솔,액고비,을순농도,미파온도이급미파시간대제취솔적영향。이차회귀통용선전조합설계적최우공예조건시:17.5배량적65%적을순용액,재65℃하용700 W적미파제취64 min。통과미파제취방법교전통적침제법구유모시단,제취솔고적특점,구유교호적응용전경。
The extraction of hypericin from hypericum perforatum by microwave was studied in this paper. With the aim of extraction rate, the microwave power, liquid to solid ratio, ethanol concentration, temperature and time were investigated in the single factor experiment and the Quadratic general rotary unitized design. The optimum extrac-tion condition as follow:17 . 5 times ethanol solution with concentration of 65%, extracted temperature is 65 degree centigrade, microwave power is 700 W, and the extraction time is 64 min. Comparing with the lixiviation, the micro-wave extraction process the advantage of consuming time short and high extraction rate, and it is with a better applica-tion prospect.