光谱学与光谱分析
光譜學與光譜分析
광보학여광보분석
SPECTROSCOPY AND SPECTRAL ANALYSIS
2014年
10期
2764-2768
,共5页
束茹欣%蔡嘉月%杨征宇%杨凯%赵龙莲%张录达%张晔晖%李军会
束茹訢%蔡嘉月%楊徵宇%楊凱%趙龍蓮%張錄達%張曄暉%李軍會
속여흔%채가월%양정우%양개%조룡련%장록체%장엽휘%리군회
烟叶%风格%近红外光谱
煙葉%風格%近紅外光譜
연협%풍격%근홍외광보
Tobacco%Style features%Near-infrared spectroscopy
以在2003年-2012年向国内17个主要烤烟产地,五大烟叶生态产区,收集的4733个烟叶样品的近红外光谱为试验对象,其中浓香型烟叶光谱1580条,清香型2004条,中间香型1149条;应用基于主成分及Fisher准则(PPF)的方法建立烟叶生态产区和风格特征的投影分析模型,以生态产区模型的分析结果阐释了烟叶香型风格划分的合理性,并依据风格特征模型得到的预测样品投影值与模型中各类投影均值之间的欧氏距离,对预测样品给出最近和次近类别及描述风格特征程度的量化分值,结合模型中各类投影值的离散度以及设定阈值,将预测结果细化为典型浓、浓偏中、中偏浓、典型中、中偏清、清偏中、典型清、清透浓、浓透清等9类或超模型范围样品;应用2102在实际复烤生产加工及各烟叶原料基地中收集的不同部位、不同产地的35个烟叶样品验证了分析结果的合理性。该种分析方式,不仅可以实现预测样品的判别分析,并且可得到关于预测样品更细化的风格特征信息,可对烟草工业企业实现原料的跨区组合及叶组配方等提供指导。
以在2003年-2012年嚮國內17箇主要烤煙產地,五大煙葉生態產區,收集的4733箇煙葉樣品的近紅外光譜為試驗對象,其中濃香型煙葉光譜1580條,清香型2004條,中間香型1149條;應用基于主成分及Fisher準則(PPF)的方法建立煙葉生態產區和風格特徵的投影分析模型,以生態產區模型的分析結果闡釋瞭煙葉香型風格劃分的閤理性,併依據風格特徵模型得到的預測樣品投影值與模型中各類投影均值之間的歐氏距離,對預測樣品給齣最近和次近類彆及描述風格特徵程度的量化分值,結閤模型中各類投影值的離散度以及設定閾值,將預測結果細化為典型濃、濃偏中、中偏濃、典型中、中偏清、清偏中、典型清、清透濃、濃透清等9類或超模型範圍樣品;應用2102在實際複烤生產加工及各煙葉原料基地中收集的不同部位、不同產地的35箇煙葉樣品驗證瞭分析結果的閤理性。該種分析方式,不僅可以實現預測樣品的判彆分析,併且可得到關于預測樣品更細化的風格特徵信息,可對煙草工業企業實現原料的跨區組閤及葉組配方等提供指導。
이재2003년-2012년향국내17개주요고연산지,오대연협생태산구,수집적4733개연협양품적근홍외광보위시험대상,기중농향형연협광보1580조,청향형2004조,중간향형1149조;응용기우주성분급Fisher준칙(PPF)적방법건립연협생태산구화풍격특정적투영분석모형,이생태산구모형적분석결과천석료연협향형풍격화분적합이성,병의거풍격특정모형득도적예측양품투영치여모형중각류투영균치지간적구씨거리,대예측양품급출최근화차근유별급묘술풍격특정정도적양화분치,결합모형중각류투영치적리산도이급설정역치,장예측결과세화위전형농、농편중、중편농、전형중、중편청、청편중、전형청、청투농、농투청등9류혹초모형범위양품;응용2102재실제복고생산가공급각연협원료기지중수집적불동부위、불동산지적35개연협양품험증료분석결과적합이성。해충분석방식,불부가이실현예측양품적판별분석,병차가득도관우예측양품경세화적풍격특정신식,가대연초공업기업실현원료적과구조합급협조배방등제공지도。
In the present paper ,a total of 4 733 flue-cured tobacco samples collected from 2003 to 2012 in 17 provincial origins and 5 ecological areas were tested by near infrared spectroscopy ,including the NONG (Luzhou) flavor 1 580 cartons ,QING (Fen) flavor 2004 cartons and Intermediate flavor 1 149 cartons .Using projection model based on principal component and Fish-er criterion (PPF) ,Projection analysis models of tobacco ecological regions and style characteristics were established .Reasona-bleness of style flavor division is illustrated by the model results of tobacco ecological areas .With the Euclidean distance between the predicted sample projection values and the mean projection values of each class in style characteristics model ,a description is given for the prediction samples to quantify the extent of the style features ,and their first and second close categories .Using the dispersion of projected values in model and the given threshold value ,prediction results can be refined into typical NONG , NONG to Intermediate ,Intermediate to NONG ,typical Intermediate ,Intermediate to QING ,QING to Intermediate ,typical QING ,QINGto NONG ,NONG to QING ,or super-model range .The model was validated by 35 tobacco samples obtained from the re-dryingprocess in 2012 with different origins and parts .This kind of analysis methods not only can achieve discriminant analysis ,but also can get richer feature attribute information and provide guidance to raw tobacco processing and formulations .