陶瓷学报
陶瓷學報
도자학보
JOURNAL OF CERAMICS
2014年
3期
309-313
,共5页
羧甲基壳聚糖%膨润土%复合材料%吸附
羧甲基殼聚糖%膨潤土%複閤材料%吸附
최갑기각취당%팽윤토%복합재료%흡부
carboxymethyl chitosan%bentonite%composite materials%adsorption
以一氯乙酸、壳聚糖、氢氧化钠为主要原料了制备N-羧甲基壳聚糖,并将其负载于膨润土上,制备得到了羧甲基壳聚糖/膨润土复合材料。利用红外(IR)、扫描电镜(SEM)对复合材料进行了表征。通过复合材料对亚甲基蓝溶液的吸附性能实验,优化出最佳吸附条件为30℃下,pH=8,亚甲基蓝溶液的初始浓度为6 mg/L时的吸附效果最好,达86.80%。
以一氯乙痠、殼聚糖、氫氧化鈉為主要原料瞭製備N-羧甲基殼聚糖,併將其負載于膨潤土上,製備得到瞭羧甲基殼聚糖/膨潤土複閤材料。利用紅外(IR)、掃描電鏡(SEM)對複閤材料進行瞭錶徵。通過複閤材料對亞甲基藍溶液的吸附性能實驗,優化齣最佳吸附條件為30℃下,pH=8,亞甲基藍溶液的初始濃度為6 mg/L時的吸附效果最好,達86.80%。
이일록을산、각취당、경양화납위주요원료료제비N-최갑기각취당,병장기부재우팽윤토상,제비득도료최갑기각취당/팽윤토복합재료。이용홍외(IR)、소묘전경(SEM)대복합재료진행료표정。통과복합재료대아갑기람용액적흡부성능실험,우화출최가흡부조건위30℃하,pH=8,아갑기람용액적초시농도위6 mg/L시적흡부효과최호,체86.80%。
N-carboxymethyl chitosan was prepared by using chloroacetic acid, chitosan, and sodium hydroxide as the main raw material, and then carboxymethyl chitosan/Bentonite composite materials loaded on the bentonite was prepared. Infra-red spectrum(IR) and Scanning Electron Microscope(SEM)techniques were ued to characterize the carboxymethyl chitosan/Bentonite composite material. The adsorption test of carboxymethyl chitosan/Bentonite composite materials for Methylene blue solution was investigated. The researches of the exeperimenial results show htat:When the temperature 30℃, pH equals 8, and the initial concentration of methylene blue solution of 6 mg/L, the adsorption of rate is 86.80%.