粮食与油脂
糧食與油脂
양식여유지
CEREALS & OILS
2014年
7期
10-13
,共4页
淀粉微球%姜黄素%吸附性
澱粉微毬%薑黃素%吸附性
정분미구%강황소%흡부성
starch microsphere%curcumin%adsorption
采用反相悬浮法合成淀粉微球作用于姜黄素吸附量的最佳工艺条件。通过单因素实验和Plackett-Burman试验确定了交联剂用量、油水比例、合成温度和乳化剂用量对姜黄素吸附量的影响,根据中心组合设计原理采用四因素三水平的响应面分析法,得到淀粉微球吸附姜黄素的最佳工艺条件。结果表明,淀粉微球吸附姜黄素的最佳条件:交联剂用量为5.5 mL,油水比例为4.01∶1,反应温度为45.1℃,乳化剂用量为0.5 g,姜黄素吸附量预测值为1.228 mg/g,验证值为1.259 mg/g,与预测值的相对误差为0.031 mg/g。
採用反相懸浮法閤成澱粉微毬作用于薑黃素吸附量的最佳工藝條件。通過單因素實驗和Plackett-Burman試驗確定瞭交聯劑用量、油水比例、閤成溫度和乳化劑用量對薑黃素吸附量的影響,根據中心組閤設計原理採用四因素三水平的響應麵分析法,得到澱粉微毬吸附薑黃素的最佳工藝條件。結果錶明,澱粉微毬吸附薑黃素的最佳條件:交聯劑用量為5.5 mL,油水比例為4.01∶1,反應溫度為45.1℃,乳化劑用量為0.5 g,薑黃素吸附量預測值為1.228 mg/g,驗證值為1.259 mg/g,與預測值的相對誤差為0.031 mg/g。
채용반상현부법합성정분미구작용우강황소흡부량적최가공예조건。통과단인소실험화Plackett-Burman시험학정료교련제용량、유수비례、합성온도화유화제용량대강황소흡부량적영향,근거중심조합설계원리채용사인소삼수평적향응면분석법,득도정분미구흡부강황소적최가공예조건。결과표명,정분미구흡부강황소적최가조건:교련제용량위5.5 mL,유수비례위4.01∶1,반응온도위45.1℃,유화제용량위0.5 g,강황소흡부량예측치위1.228 mg/g,험증치위1.259 mg/g,여예측치적상대오차위0.031 mg/g。
The optimal synthesis conditions using inverse suspension starch microspheres role in the adsorption capacity of curcumin. By single factor test and Plackett-Burman test to determine the effect of crosslinker dosage,oil-water ratio,reaction temperature and emulsifier dosage impact on adsorption capacity of curcumin. According to the principle of central composite design with four factors and three levels of response surface analysis,the optimum conditions of starch microspheres absorption of curcumin. The results showed that starch microspheres optimal conditions for the absorption curcumin were as follows:crosslinker dosage was 5.5 mL,oil-water ratio was 4.01∶1,reaction temperature was 45.1℃and emulsifier was 0.5 g.The predicted adsorption yield was 1.228 mg/g,while the actual adsorption yield was 1.259 mg/g,with relative error of 0.031 mg/g.