CAJ | 학술논문

目的：对制何首乌颗粒进行质量控制考察。方法：采用TLC法对处方中的制何首乌进行定性鉴别，用HPLC法测定制何首乌中二苯乙烯苷的含量。结果：在TLC 图谱中能检出制何首乌，二苯乙烯苷在0.0296g/L-0.148g/L的范围内线性良好（r＝0.9942），平均加样回收率为99.63％，RSD 为1.1％。结论：所建立方法简便可行，重现性好，可用于制何首乌颗粒的质量控制。
목적：대제하수오과립진행질량공제고찰。방법：채용TLC법대처방중적제하수오진행정성감별，용HPLC법측정제하수오중이분을희감적함량。결과：재TLC 도보중능검출제하수오，이분을희감재0.0296g/L-0.148g/L적범위내선성량호（r＝0.9942），평균가양회수솔위99.63％，RSD 위1.1％。결론：소건립방법간편가행，중현성호，가용우제하수오과립적질량공제。
Objective Investigate Prepared fleeceflower root granule quality.Methods Prepared fleeceflower root was identified by TLC,and content of 2,3,5,4'-tetera-hydroxystilbene -2 -O-β-D-glucoside was determined by HPLC.Results Prepared fleeceflower root could be identified by TLC.2,3,5,4'-tetera-hydroxystilbene-2-O-β-D-glucoside showed a good linear re-lationship at a range of 0.0296g/L-0.148g/L (r=0.9942),the average recovery was 99.63%,and RSD was 1.1%.Conclusion The established method is simple,feasible and reproducible and it can be used as the quality standards for Prepared fleeceflower root granule.