中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
4期
565-567
,共3页
胡北%马宏达%孙学惠%张晋%史国兵
鬍北%馬宏達%孫學惠%張晉%史國兵
호북%마굉체%손학혜%장진%사국병
和肝利胆颗粒%黄芩苷%正交试验%高效液相色谱
和肝利膽顆粒%黃芩苷%正交試驗%高效液相色譜
화간리담과립%황금감%정교시험%고효액상색보
Hegan Lidan granules%Baicalin%Orthogonal design%HPLC
目的:优选和肝利胆颗粒最佳提取工艺条件。方法:以加水量、提取时间和提取次数为考察因素,以黄芩苷含量和浸膏得率为评价指标,采用正交试验优选最佳工艺条件。结果:最佳工艺条件为加8倍量水,提取3次,每次2h。结论:该提取工艺稳定可行,可用于和肝利胆颗粒的提取。
目的:優選和肝利膽顆粒最佳提取工藝條件。方法:以加水量、提取時間和提取次數為攷察因素,以黃芩苷含量和浸膏得率為評價指標,採用正交試驗優選最佳工藝條件。結果:最佳工藝條件為加8倍量水,提取3次,每次2h。結論:該提取工藝穩定可行,可用于和肝利膽顆粒的提取。
목적:우선화간리담과립최가제취공예조건。방법:이가수량、제취시간화제취차수위고찰인소,이황금감함량화침고득솔위평개지표,채용정교시험우선최가공예조건。결과:최가공예조건위가8배량수,제취3차,매차2h。결론:해제취공예은정가행,가용우화간리담과립적제취。
Objective:To optimize the extraction process of Hegan Lidan granules. Methods:In order to choose the optimal tech-nological parameters, the content of baicalin was determined by HPLC. An orthogonal method was utilized with solvent volume, extrac-tion time and extraction times as the impacting factors and the content of baicalin and extraction rate as the indices. Results:The opti-mal parameters were as follows:using 8-fold water as the solvent, the raw material was extracted three times with 2 h for each. Con-clusion:The process is steady and feasible, and can be used in the extraction of Hegan Lidan granules.