化学与粘合
化學與粘閤
화학여점합
CHEMISTRY AND ADHESION
2014年
3期
199-201
,共3页
有机硅烷偶联剂%“三防”保护涂料%紫外荧光
有機硅烷偶聯劑%“三防”保護塗料%紫外熒光
유궤규완우련제%“삼방”보호도료%자외형광
Silane coupling agent%three proofings protective coating%UV fluorescence
以硅烷偶联剂、甲基丙烯酸酯类、甲基丙烯酸、引发剂（BPO）、溶剂、荧光粉等为原料，采用溶剂聚合方法合成三防保护剂系列涂料。考察了反应温度、引发反应的诱导期、引发剂的用量等对涂料性能的影响。经正交试验确定了最佳工艺条件：反应温度80±5℃，反应的诱导期控制在50min，引发剂的用量为投料量0.57%，可见荧光粉用量为0.25%。
以硅烷偶聯劑、甲基丙烯痠酯類、甲基丙烯痠、引髮劑（BPO）、溶劑、熒光粉等為原料，採用溶劑聚閤方法閤成三防保護劑繫列塗料。攷察瞭反應溫度、引髮反應的誘導期、引髮劑的用量等對塗料性能的影響。經正交試驗確定瞭最佳工藝條件：反應溫度80±5℃，反應的誘導期控製在50min，引髮劑的用量為投料量0.57%，可見熒光粉用量為0.25%。
이규완우련제、갑기병희산지류、갑기병희산、인발제（BPO）、용제、형광분등위원료，채용용제취합방법합성삼방보호제계렬도료。고찰료반응온도、인발반응적유도기、인발제적용량등대도료성능적영향。경정교시험학정료최가공예조건：반응온도80±5℃，반응적유도기공제재50min，인발제적용량위투료량0.57%，가견형광분용량위0.25%。
A three proofings protective coating is synthesized by means of solvent polymerization method with using methacrylate esters, silane coupling agent, initiator(BPO), solvents and fluorescent powder as raw materials. The effects of reaction temperature, induction period of initiating the reaction and the dosage of initiator on the performances of the coating are investigated. By the orthogonal test, the optimum process conditions are confirmed as follows: the reaction temperature is 80 ±5℃, the induction period of reaction is controlled in 50mins, and the dosage of initiator is 0.57%of feed, and the visible fluorescent powder dosage is 0.25%.
