化学与粘合
化學與粘閤
화학여점합
CHEMISTRY AND ADHESION
2014年
3期
188-190
,共3页
巩桂芬%吴谙宇%朱丽娜%王晓惠
鞏桂芬%吳諳宇%硃麗娜%王曉惠
공계분%오암우%주려나%왕효혜
材料学%纤维素%微波
材料學%纖維素%微波
재료학%섬유소%미파
Material science%cellulose%microwave
采用纤维素为原料,以离子液体为溶剂,在微波辐射下进行纤维素的预处理。预处理完成后进行再生纤维素的酶解产糖,并采用DNS分光光度计法进行还原糖产率的测定,进而分析微波功率与时间对再生纤维素还原糖产率的影响。还原糖转化率最佳值(96.21%)出现在微波功率为230W处理5min时;稻杆产糖量随着微波时间的延长而呈现先上升后下降的趋势;在较强的功率539W条件下,延长作用时间则会引起还原糖转化率的上升,但继续延长时间,溶剂完全喷溅,难以继续进行处理。
採用纖維素為原料,以離子液體為溶劑,在微波輻射下進行纖維素的預處理。預處理完成後進行再生纖維素的酶解產糖,併採用DNS分光光度計法進行還原糖產率的測定,進而分析微波功率與時間對再生纖維素還原糖產率的影響。還原糖轉化率最佳值(96.21%)齣現在微波功率為230W處理5min時;稻桿產糖量隨著微波時間的延長而呈現先上升後下降的趨勢;在較彊的功率539W條件下,延長作用時間則會引起還原糖轉化率的上升,但繼續延長時間,溶劑完全噴濺,難以繼續進行處理。
채용섬유소위원료,이리자액체위용제,재미파복사하진행섬유소적예처리。예처리완성후진행재생섬유소적매해산당,병채용DNS분광광도계법진행환원당산솔적측정,진이분석미파공솔여시간대재생섬유소환원당산솔적영향。환원당전화솔최가치(96.21%)출현재미파공솔위230W처리5min시;도간산당량수착미파시간적연장이정현선상승후하강적추세;재교강적공솔539W조건하,연장작용시간칙회인기환원당전화솔적상승,단계속연장시간,용제완전분천,난이계속진행처리。
The cellulose is pretreated under microwave radiation with using cellulose as raw material and ionic liquids as solvents. After the pre-treatment, the regenerated cellulose(RE) is enzymatic hydrolysed to produce sugar and the DNS spectro-photometric method is used to determine the yield of reducing sugar. And then the effect of microwave power and time on the yield of reducing sugar is analyzed which is produced from regenerat-ed celluloses. When the RE is treated for 5min under a microwave power of 230W, the reducing sugar conversion rate reaches highest which is 96.21%; The yield of sugar produced from rice straw firstly increases and then declines with lengthening the microwave time; Under the microwave radiation with a strong power of 539W, extending microwave radiation time will lead to a higher conversion rate of reducing sugar, however continue extending the time will result in completely solvent spill and difficult to process.