化学与粘合
化學與粘閤
화학여점합
CHEMISTRY AND ADHESION
2014年
3期
162-166
,共5页
杨威%王丽%王玮%车春波%李俊生%左金龙
楊威%王麗%王瑋%車春波%李俊生%左金龍
양위%왕려%왕위%차춘파%리준생%좌금룡
植物药提取废渣%有效成分%微波提取%正交实验
植物藥提取廢渣%有效成分%微波提取%正交實驗
식물약제취폐사%유효성분%미파제취%정교실험
Extractive residue of Chinese herbal medicine%active components%microwave-assisted extraction%orthogonal experiment
利用微波萃取技术针对某中药厂双黄连制剂生产过程中产生的废弃黄芩提取药渣进行了有效成分的再次提取并同传统水提工艺进行了对比。以有效成分(黄芩苷)收率做为考察指标,用正交设计结合单因素分析方法考察微波提取黄芩苷的最佳提取条件,旨在探讨植物药提取废渣的再利用价值、探寻植物药提取废渣资源化的有效途径。结果表明:各因素对黄芩苷收率的影响依次为:乙醇浓度>粒径>功率>提取时间,其中乙醇浓度为显著性影响因素,最佳工艺为:以30%乙醇作为提取溶剂,黄芩药渣粒径80目,微波功率选择500W,微波提取2min。与水提工艺相比,在最佳工艺条件下,微波提取工艺能够获得较高收率的黄芩苷。
利用微波萃取技術針對某中藥廠雙黃連製劑生產過程中產生的廢棄黃芩提取藥渣進行瞭有效成分的再次提取併同傳統水提工藝進行瞭對比。以有效成分(黃芩苷)收率做為攷察指標,用正交設計結閤單因素分析方法攷察微波提取黃芩苷的最佳提取條件,旨在探討植物藥提取廢渣的再利用價值、探尋植物藥提取廢渣資源化的有效途徑。結果錶明:各因素對黃芩苷收率的影響依次為:乙醇濃度>粒徑>功率>提取時間,其中乙醇濃度為顯著性影響因素,最佳工藝為:以30%乙醇作為提取溶劑,黃芩藥渣粒徑80目,微波功率選擇500W,微波提取2min。與水提工藝相比,在最佳工藝條件下,微波提取工藝能夠穫得較高收率的黃芩苷。
이용미파췌취기술침대모중약엄쌍황련제제생산과정중산생적폐기황금제취약사진행료유효성분적재차제취병동전통수제공예진행료대비。이유효성분(황금감)수솔주위고찰지표,용정교설계결합단인소분석방법고찰미파제취황금감적최가제취조건,지재탐토식물약제취폐사적재이용개치、탐심식물약제취폐사자원화적유효도경。결과표명:각인소대황금감수솔적영향의차위:을순농도>립경>공솔>제취시간,기중을순농도위현저성영향인소,최가공예위:이30%을순작위제취용제,황금약사립경80목,미파공솔선택500W,미파제취2min。여수제공예상비,재최가공예조건하,미파제취공예능구획득교고수솔적황금감。
Extracting active component from Chinese herbal medicine extractive residue which came from a traditional Chinese medicine plant was carried out by means of microwave-assisted extraction and the technique was compared with the traditional one (aqueous extraction). In order to discuss the recycle value of extracting from the extracted Chinese herbal residue, and to seek for the efficient path for recycling of Chinese herbal residue, the process for extracting baicalin was optimized with using yield of baicalin as the investigation index by means of single factor analysis and orthogonal experiments. The results showed influence factors on baicalin yield as follows(form great to less):ethanol concentration>granularity of ex-tractive residue>microwave power>duration of microwave irradiation. And the ethanol concentration was the significant influencing factor. The opti-mal parameters were obtained as follows:30%ethanol was chosen as the extraction solvent;the microwave power was 500W;the granularity of the ex-traction residue was 80 meshes;the duration of microwave irradiation was 2min. The higher yield of baicalin could be achieved by microwave-assisted extraction.