标准科学
標準科學
표준과학
STANDARD SCIENCE
2014年
3期
52-54
,共3页
郭盈岑%农馥俏%干宁军
郭盈岑%農馥俏%榦寧軍
곽영잠%농복초%간저군
甘蔗%乐果%特丁磷%农药残留%高效液相色谱串联四级杆线性离子阱质谱
甘蔗%樂果%特丁燐%農藥殘留%高效液相色譜串聯四級桿線性離子阱質譜
감자%악과%특정린%농약잔류%고효액상색보천련사급간선성리자정질보
sugarcane%pesticide residue%Dimethoate%Terbufos%ASE-HPLC-MS/MS
本文建立了甘蔗中乐果、特丁磷农药残留的加速溶剂萃取-高效液相色谱串联四级杆线性离子阱质谱（ASE-HPLC-MS/MS-QTRAP）检测方法。该方法样品前处理简单、快速，分析时间短，灵敏度、准确度和精密度均符合农药痕量分析的需要，满足甘蔗中有机磷农药残留检测要求。
本文建立瞭甘蔗中樂果、特丁燐農藥殘留的加速溶劑萃取-高效液相色譜串聯四級桿線性離子阱質譜（ASE-HPLC-MS/MS-QTRAP）檢測方法。該方法樣品前處理簡單、快速，分析時間短，靈敏度、準確度和精密度均符閤農藥痕量分析的需要，滿足甘蔗中有機燐農藥殘留檢測要求。
본문건립료감자중악과、특정린농약잔류적가속용제췌취-고효액상색보천련사급간선성리자정질보（ASE-HPLC-MS/MS-QTRAP）검측방법。해방법양품전처리간단、쾌속，분석시간단，령민도、준학도화정밀도균부합농약흔량분석적수요，만족감자중유궤린농약잔류검측요구。
In the paper, a method is developed for the determination of dimethoate and terbufos pesticide residues in sugarcane by accelerated solvent extraction high performance liquid chromatography tandem mass spectrometry (ASE-HPLC-MS/MS). The method is simple, rapid and characterized with acceptable sensitivity and accuracy to meet the requirements of the pesticide residue analysis. This procedure is suitable for the determination of dimethoate and terbufos pesticide residues in sugarcane.
