中医药学报
中醫藥學報
중의약학보
ACTA CHINESE MEDICINE AND PHARMACOLOGY
2014年
2期
67-70
,共4页
徐士勋%邢延一%林锦旋%周燊%绪扩%韩秋俊%雷海民
徐士勛%邢延一%林錦鏇%週燊%緒擴%韓鞦俊%雷海民
서사훈%형연일%림금선%주신%서확%한추준%뢰해민
醋炙%鳖甲%总氨基酸%提取工艺
醋炙%鱉甲%總氨基痠%提取工藝
작자%별갑%총안기산%제취공예
Vinegar moxibustion%Carapax Trionycis%Total amino acids%Processing
目的：优选醋炙鳖甲总氨基酸提取工艺。方法：以浸膏得率和总氨基酸含量为指标，对提取方法和提取溶剂进行优选，采用正交试验法考察该方法下提取鳖甲的溶剂用量、提取时间和提取次数，优化工艺条件。结果：以蒸馏水为溶剂进行回流法提取时，最佳提取工艺为10倍水煎煮2 h，提取3次。结论：以蒸馏水为溶剂进行回流提取时，浸膏得率和总氨基酸含量均较高，该方法设计合理、简便易行。
目的：優選醋炙鱉甲總氨基痠提取工藝。方法：以浸膏得率和總氨基痠含量為指標，對提取方法和提取溶劑進行優選，採用正交試驗法攷察該方法下提取鱉甲的溶劑用量、提取時間和提取次數，優化工藝條件。結果：以蒸餾水為溶劑進行迴流法提取時，最佳提取工藝為10倍水煎煮2 h，提取3次。結論：以蒸餾水為溶劑進行迴流提取時，浸膏得率和總氨基痠含量均較高，該方法設計閤理、簡便易行。
목적：우선작자별갑총안기산제취공예。방법：이침고득솔화총안기산함량위지표，대제취방법화제취용제진행우선，채용정교시험법고찰해방법하제취별갑적용제용량、제취시간화제취차수，우화공예조건。결과：이증류수위용제진행회류법제취시，최가제취공예위10배수전자2 h，제취3차。결론：이증류수위용제진행회류제취시，침고득솔화총안기산함량균교고，해방법설계합리、간편역행。
Objective:To optimizie the extracting technology of the total amino acids in Carapax Trionycis stir -frying with vinegar .Methods:Use the rate of extractum and the contents of total amino as the index to optimize the extracting meth-od and the extracting solvent , then utilize the orthogonal experiments to evaluate the factors ( the ratio of the solvent ,the time of extraction and the frequency of extraction ) to optimize the technology .Results: The best technology was to ex-tract the Carapax Trionycis stir -frying with vinegar by using 10 times ’ water lasted 2 hours for 3 times by the reflux method with the water as the solvent .Conclusion:When using the reflux method with the distilled water as the solvent , the rate of extractum and the contents of total amino acids are both the highest , so the procedure is convenient , appropri-ate and feasible .
