山东农业科学
山東農業科學
산동농업과학
SHANGDONG AGRICULTURAL SCIENCES
2014年
5期
122-126
,共5页
范臖%王明林%于建垒%宋国春%李瑞娟
範臖%王明林%于建壘%宋國春%李瑞娟
범흥%왕명림%우건루%송국춘%리서연
霜脲氰%喹啉铜%黄瓜%残留%风险评估
霜脲氰%喹啉銅%黃瓜%殘留%風險評估
상뇨청%규람동%황과%잔류%풍험평고
Cymoxanil%Oxine-copper%Cucumber%Residue%Risk assessment
为了探明霜脲氰和喹啉铜在黄瓜上的残留特性和使用安全性,采用高效液相色谱分析技术测定了霜脲氰和喹啉铜在黄瓜中的残留动态和最终残留。结果表明:霜脲氰和喹啉铜在黄瓜中的半衰期分别为1.8~2.5 d和2.6~4.1 d。以40%霜脲氰·喹啉铜悬浮剂360、540 g a.i./hm2,于黄瓜生长期连续喷药3、4次,最后一次施药后1、2、3、5 d,黄瓜中霜脲氰残留量均低于0.5 mg/kg(MRL),喹啉铜残留量均低于2.0 mg/kg(MRL)。膳食风险评估结果表明,霜脲氰和喹啉铜的风险商值仅为0.62%和0.40%,处于安全水平。推荐该药在黄瓜上应用的安全间隔期为1d。
為瞭探明霜脲氰和喹啉銅在黃瓜上的殘留特性和使用安全性,採用高效液相色譜分析技術測定瞭霜脲氰和喹啉銅在黃瓜中的殘留動態和最終殘留。結果錶明:霜脲氰和喹啉銅在黃瓜中的半衰期分彆為1.8~2.5 d和2.6~4.1 d。以40%霜脲氰·喹啉銅懸浮劑360、540 g a.i./hm2,于黃瓜生長期連續噴藥3、4次,最後一次施藥後1、2、3、5 d,黃瓜中霜脲氰殘留量均低于0.5 mg/kg(MRL),喹啉銅殘留量均低于2.0 mg/kg(MRL)。膳食風險評估結果錶明,霜脲氰和喹啉銅的風險商值僅為0.62%和0.40%,處于安全水平。推薦該藥在黃瓜上應用的安全間隔期為1d。
위료탐명상뇨청화규람동재황과상적잔류특성화사용안전성,채용고효액상색보분석기술측정료상뇨청화규람동재황과중적잔류동태화최종잔류。결과표명:상뇨청화규람동재황과중적반쇠기분별위1.8~2.5 d화2.6~4.1 d。이40%상뇨청·규람동현부제360、540 g a.i./hm2,우황과생장기련속분약3、4차,최후일차시약후1、2、3、5 d,황과중상뇨청잔류량균저우0.5 mg/kg(MRL),규람동잔류량균저우2.0 mg/kg(MRL)。선식풍험평고결과표명,상뇨청화규람동적풍험상치부위0.62%화0.40%,처우안전수평。추천해약재황과상응용적안전간격기위1d。
In order to study the residual characteristics and use security of cymoxanil and oxine-copper in cucumber,the residual dynamics and final residue were determined by HPLC.The results showed that the half-life of cymoxanil and oxine-copper in cucumber were 1 .8~2.5 days and 2.6~4.1 days respectively. Spraying 3 or 4 times during growing period of cucumber with 360 or 540 g a.i./hm2 of 40% cymoxanil and oxine-copper SC,the residue of cymoxanil and oxine-copper in cucumber after the last application for 1 ,2, 3 and 5 days were all lower than 0.5 mg/kg (MRL)and 2 mg/kg (MRL)respectively.The dietary risk as-sessment showed that the value at risk of cymoxanil and oxine-copper were 0.62%and 0.40%,which were in the security levels.It suggested that the pre-harvest interval of cymoxanil and oxine-copper in cucumber was 1 day.