湖州师范学院学报
湖州師範學院學報
호주사범학원학보
JOURNAL OF HUZHOU TEACHERS COLLEGE
2014年
4期
27-32
,共6页
孙来玉%尹莉%姚婷%杨金田%邵朝纲%钱坤
孫來玉%尹莉%姚婷%楊金田%邵朝綱%錢坤
손래옥%윤리%요정%양금전%소조강%전곤
克伦特罗%样品前处理%残留检测
剋倫特囉%樣品前處理%殘留檢測
극륜특라%양품전처리%잔류검측
clenbuterol%sample pre treatment%residue detection
介绍了盐酸克伦特罗残留检测的样品前处理技术、分析测试方法,并绘制了样品前处理技术路线图。其样品前处理技术主要有沉淀、离心、液液萃取、固相萃取、基体分散固相萃取、中空纤维液相微萃取、分散液相微萃取、固相微萃取、免疫亲和色谱、分子印迹、超临界萃取等。分析测试方法主要有化学分析法、色谱法、毛细管电泳法、电化学分析法、免疫学分析法、生物传感器法等。相对于色谱质谱联用等仪器分析技术的高速发展,盐酸克伦特罗残留检测样品前处理技术发展较为缓慢。因此,发展快速、高效、高选择性、环境友好、易于标准化且与分析测试方法衔接配套的样品前处理技术非常重要。
介紹瞭鹽痠剋倫特囉殘留檢測的樣品前處理技術、分析測試方法,併繪製瞭樣品前處理技術路線圖。其樣品前處理技術主要有沉澱、離心、液液萃取、固相萃取、基體分散固相萃取、中空纖維液相微萃取、分散液相微萃取、固相微萃取、免疫親和色譜、分子印跡、超臨界萃取等。分析測試方法主要有化學分析法、色譜法、毛細管電泳法、電化學分析法、免疫學分析法、生物傳感器法等。相對于色譜質譜聯用等儀器分析技術的高速髮展,鹽痠剋倫特囉殘留檢測樣品前處理技術髮展較為緩慢。因此,髮展快速、高效、高選擇性、環境友好、易于標準化且與分析測試方法銜接配套的樣品前處理技術非常重要。
개소료염산극륜특라잔류검측적양품전처리기술、분석측시방법,병회제료양품전처리기술로선도。기양품전처리기술주요유침정、리심、액액췌취、고상췌취、기체분산고상췌취、중공섬유액상미췌취、분산액상미췌취、고상미췌취、면역친화색보、분자인적、초림계췌취등。분석측시방법주요유화학분석법、색보법、모세관전영법、전화학분석법、면역학분석법、생물전감기법등。상대우색보질보련용등의기분석기술적고속발전,염산극륜특라잔류검측양품전처리기술발전교위완만。인차,발전쾌속、고효、고선택성、배경우호、역우표준화차여분석측시방법함접배투적양품전처리기술비상중요。
This paper reviews the analytical methods and sample pre treatment techniques of clen-buterol residue detection.The technical routes of sample pre treatment are plotted.Sample pre treat-ment techniques mainly include precipitation,centrifugation,liquid liquid extraction,solid phase ex-traction ,matrix solid phase dispersion,hollow fiber liquid phase micro extraction ,dispersive liq-uid liquid micro extraction,solid phase micro extraction,immunoaffinity chromatography,molecu-lar imprinted polymer,supercritical fluid extraction,etc.Analytical methods mainly include chemical a-nalysis,chromatography,capillary electrophoresis,immunoassay,electrochemical analysis,biosensor, etc.Relative to the rapid development of chromatography mass spectrometry hyphenated techniques and other instrumental analysis techniques,sample pre treatment of clenbuterol hydrochloride residue detection development is relatively slow,and therefore,the development of fast,efficient,highly selec-tive,environmentally friendly,easy and standardized sample pre treatment technology is very impor-tant.