化学研究
化學研究
화학연구
CHEMICAL RESEARCHES
2014年
3期
221-228
,共8页
曹刘琴%冷春丽%李园园%赵彦保%李宾杰
曹劉琴%冷春麗%李園園%趙彥保%李賓傑
조류금%랭춘려%리완완%조언보%리빈걸
铜树枝晶%水热合成%结构表征%抗菌性能%评价
銅樹枝晶%水熱閤成%結構錶徵%抗菌性能%評價
동수지정%수열합성%결구표정%항균성능%평개
copper dendrite%hydrothermal synthesis%structure characterization%antibacterial performance%evaluation
在乙醇胺-水混合溶液中采用水热处理硫酸铜的方法制备了多结构的铜树枝晶;采用X射线粉末衍射仪、扫描电子显微镜、透射电子显微镜分析了所得样品的结构和形貌;采用牛津杯法评价了其对金黄葡萄球菌、枯草芽孢杆菌、大肠杆菌和绿脓杆菌的抗菌性能。结果表明,铜树枝晶由一个长的一级中心主干和许多高度对称分布在主干两侧的二级分支结构构成,且形貌均匀;反应温度、反应时间以及溶剂组成对铜树枝晶的形貌有很大影响。与此同时,铜树枝晶表现出选择性的抗菌行为,对金黄葡萄球菌、枯草芽孢杆菌和绿脓杆菌更有效。
在乙醇胺-水混閤溶液中採用水熱處理硫痠銅的方法製備瞭多結構的銅樹枝晶;採用X射線粉末衍射儀、掃描電子顯微鏡、透射電子顯微鏡分析瞭所得樣品的結構和形貌;採用牛津杯法評價瞭其對金黃葡萄毬菌、枯草芽孢桿菌、大腸桿菌和綠膿桿菌的抗菌性能。結果錶明,銅樹枝晶由一箇長的一級中心主榦和許多高度對稱分佈在主榦兩側的二級分支結構構成,且形貌均勻;反應溫度、反應時間以及溶劑組成對銅樹枝晶的形貌有很大影響。與此同時,銅樹枝晶錶現齣選擇性的抗菌行為,對金黃葡萄毬菌、枯草芽孢桿菌和綠膿桿菌更有效。
재을순알-수혼합용액중채용수열처리류산동적방법제비료다결구적동수지정;채용X사선분말연사의、소묘전자현미경、투사전자현미경분석료소득양품적결구화형모;채용우진배법평개료기대금황포도구균、고초아포간균、대장간균화록농간균적항균성능。결과표명,동수지정유일개장적일급중심주간화허다고도대칭분포재주간량측적이급분지결구구성,차형모균균;반응온도、반응시간이급용제조성대동수지정적형모유흔대영향。여차동시,동수지정표현출선택성적항균행위,대금황포도구균、고초아포간균화록농간균경유효。
Hierarchical copper dendrites were synthesized by a facile hydrothermal treatment of copper sulfate in ethanolamine (EA )-water solution .X-ray diffraction ,scanning electron mi-croscopy ,and transmission electron microscopy analyses were employed to analyze the struc-ture and morphology of as-synthesized copper dendrites ;and their antibacterial activity against Bacillus subtilis (B .subtilis) ,Staphylococcus aureus (S .aureus) ,Escherichia coli (E .coli) and Pseudomonas aeruginosa (P .aeruginosa) was evaluated by Oxford cup method .Results indicate that as-synthesized copper dendrites have uniform morphology and consist of a long primary central stem and many highly ordered secondary branches symetrically distributed at the both sides of the stem .Reaction temperature ,reaction time ,and solvent have important effects on the morphology of copper dendrites .In the meantime ,as-synthesized copper crystals exhibit selective antibacterial performance .Namely ,they display effective antibacterial activity against S .aureus ,B .subtilis and P .aeruginosa .