CAJ | 학술논문

对 Fe52 Co34 Hf7 B6 Cu1非晶试样进行了中频磁脉冲处理,脉冲磁场频率、作用时间保持恒定：1500 Hz、10 min,脉冲磁场强度分别为15.92,19.9和23.88 kA/m。用穆斯堡尔谱(MS)和正电子湮没寿命谱(PAS)方法研究了该试样在中频磁脉冲处理前后的结构及结构缺陷变化。结果表明,在非晶合金的制备态,正电子主要在自由体积中湮没,经中频磁脉冲处理后,非晶合金发生不可逆的结构弛豫,导致湮没寿命τ1下降。随着脉冲磁场强度的增加,非晶合金发生晶化,产生新的正电子俘获中心,导致强度I2急剧增加, I1急剧降低。
대 Fe52 Co34 Hf7 B6 Cu1비정시양진행료중빈자맥충처리,맥충자장빈솔、작용시간보지항정：1500 Hz、10 min,맥충자장강도분별위15.92,19.9화23.88 kA/m。용목사보이보(MS)화정전자인몰수명보(PAS)방법연구료해시양재중빈자맥충처리전후적결구급결구결함변화。결과표명,재비정합금적제비태,정전자주요재자유체적중인몰,경중빈자맥충처리후,비정합금발생불가역적결구이예,도치인몰수명τ1하강。수착맥충자장강도적증가,비정합금발생정화,산생신적정전자부획중심,도치강도I2급극증가, I1급극강저。
The amorphous alloy specimens Fe52 Co34 Hf7 B6 Cu1 were treated by medium-frequency magnetic pulse. The treatment conditions were as follows:the pulsing magnetic field frequency and the acting time were kept at 1 500 Hz,10 min,and the field intensity were 15.92,19.9 and 23.88 kA/m respectively.The structural and structural defects of specimens before and after magnetic-pulsing were researched by M?ssbauer spectroscopy (MS)and positron annihilation lifetime spectra (PAS).The results show that in the as-quenched amorphous al-loy,the positron are mainly localized at vacancy-sized free volumes in the amorphous based phase,and the amorphous alloy produced irreversible structural relaxation after being treated by the medium-frequency mag-netic pulse which leaded to the decline of the annihilation lifetimeτ1 .With the increase of pulsing magnetic field intensity,new trapping centers of positrons are produced owing to the crystallization of amorphous phase,that leads to the intensity I 2 increases and I 1 decreases drastically.