功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
10期
10067-10071
,共5页
周佳%朱正吼%付远%乔宝英%杜康
週佳%硃正吼%付遠%喬寶英%杜康
주가%주정후%부원%교보영%두강
FeCuNbSiB 粉体%丁基橡胶%阻抗%力敏特性
FeCuNbSiB 粉體%丁基橡膠%阻抗%力敏特性
FeCuNbSiB 분체%정기상효%조항%력민특성
FeCuNbSiB powder%butyl rubber%impedance%force-sensitive properties
以粒径为45μm 的 Fe73.5 Cu1 Nb3 Si13.5 B9非晶粉体为复合相,丁基橡胶为基体相,利用模压成型法制备了粉体含量为85%、厚度为150和200μm 的复合薄膜。采用LYYL-500N高档型微机控制压力试验机对薄膜试样进行连续加载/卸载实验(速度分别为0.1,0.5和1.0 mm/min),用 TH2816LCR 数字电桥测试频率1和50 kHz下薄膜的阻抗Z 值。研究了加载/卸载速度、测试频率、薄膜厚度和环境温度对 Fe-CuNbSiB粉体/丁基橡胶力敏特性的影响。研究表明,复合薄膜在v=0.1 mm/min 时,其重复性最好,在加载过程中,应力灵敏度|k|值随着应力的增大呈现先增大后减小的变化趋势,卸载过程中,|k|值随着应力的逐渐减小而增大。在1 kHz测试频率下复合薄膜的力敏灵敏度高于50 kHz。相同测试条件下,厚度为200μm的复合薄膜的力敏灵敏性略优于150μm 的。在39.5~80℃温度范围内,随着温度的升高复合薄膜的灵敏度越高。
以粒徑為45μm 的 Fe73.5 Cu1 Nb3 Si13.5 B9非晶粉體為複閤相,丁基橡膠為基體相,利用模壓成型法製備瞭粉體含量為85%、厚度為150和200μm 的複閤薄膜。採用LYYL-500N高檔型微機控製壓力試驗機對薄膜試樣進行連續加載/卸載實驗(速度分彆為0.1,0.5和1.0 mm/min),用 TH2816LCR 數字電橋測試頻率1和50 kHz下薄膜的阻抗Z 值。研究瞭加載/卸載速度、測試頻率、薄膜厚度和環境溫度對 Fe-CuNbSiB粉體/丁基橡膠力敏特性的影響。研究錶明,複閤薄膜在v=0.1 mm/min 時,其重複性最好,在加載過程中,應力靈敏度|k|值隨著應力的增大呈現先增大後減小的變化趨勢,卸載過程中,|k|值隨著應力的逐漸減小而增大。在1 kHz測試頻率下複閤薄膜的力敏靈敏度高于50 kHz。相同測試條件下,厚度為200μm的複閤薄膜的力敏靈敏性略優于150μm 的。在39.5~80℃溫度範圍內,隨著溫度的升高複閤薄膜的靈敏度越高。
이립경위45μm 적 Fe73.5 Cu1 Nb3 Si13.5 B9비정분체위복합상,정기상효위기체상,이용모압성형법제비료분체함량위85%、후도위150화200μm 적복합박막。채용LYYL-500N고당형미궤공제압력시험궤대박막시양진행련속가재/사재실험(속도분별위0.1,0.5화1.0 mm/min),용 TH2816LCR 수자전교측시빈솔1화50 kHz하박막적조항Z 치。연구료가재/사재속도、측시빈솔、박막후도화배경온도대 Fe-CuNbSiB분체/정기상효력민특성적영향。연구표명,복합박막재v=0.1 mm/min 시,기중복성최호,재가재과정중,응력령민도|k|치수착응력적증대정현선증대후감소적변화추세,사재과정중,|k|치수착응력적축점감소이증대。재1 kHz측시빈솔하복합박막적력민령민도고우50 kHz。상동측시조건하,후도위200μm적복합박막적력민령민성략우우150μm 적。재39.5~80℃온도범위내,수착온도적승고복합박막적령민도월고。
Composite film was prepared by molding method with amorphous Fe73.5 Cu1 Nb3 Si13.5 B9 powder as compound phase and butyl rubber as matrix phase.The particle size was 45μm,the content of powder was 85%and the thickness of film was 150 or 200μm.LYYL-500N high-grade type microcomputer control pressure tes-ting machine was used to conduct program control loading with speed of 0.1,0.5 and 1.0 mm/min.Values of impedance,Z,under pressure stress were measured by TH2816LCR digital bridge with 1 and 50 kHz.The pa-per study the effect of loading speed,testing frequency,film thickness and testing temperature on force-sensi-tive properties.The results show the force-sensitive stability property was best,when the loading speed was 0. 1 mm/min.The sensitivity (|k|)of composite films increase firstly then decrease with the increasing stress during loading process,while it increase with the decreasing stress during uploading process.While the fre-quency was 1 kHz,the force-sensitive sensitivity of composite films are better than 50 kHz.The force-sensitive sensitivity of 200μm process are superior to 150μm.The higher temperature is,the better sensitivity of com-posite film is.