应用化工
應用化工
응용화공
APPLIED CHEMICAL INDUSTRY
2014年
5期
874-876
,共3页
唐晓东%李斌%李晶晶%卿大咏%张洋勇%邓杰义
唐曉東%李斌%李晶晶%卿大詠%張洋勇%鄧傑義
당효동%리빈%리정정%경대영%장양용%산걸의
油砂%溶剂%萃取%EOSA%收率
油砂%溶劑%萃取%EOSA%收率
유사%용제%췌취%EOSA%수솔
oil sands%solvents%extraction%EOSA%yield
以克拉玛依油砂为实验对象,考察石油醚、环己烷、正戊烷、正庚烷、甲苯、CS2及复合溶剂 EOSA 萃取分离油砂沥青的效果,确定 EOSA 为最佳萃取溶剂。研究了温度、溶剂用量、时间对 EOSA 萃取分离油砂沥青收率的影响。结果表明,在萃取温度30℃、剂砂比2 mL/ g 条件下萃取30 min,油砂沥青的收率可达95%以上。再生实验结果表明,在60~80℃条件下,溶剂回收率超过99%。该工艺具有无水参与、零排放、低能耗、高收率等优点。
以剋拉瑪依油砂為實驗對象,攷察石油醚、環己烷、正戊烷、正庚烷、甲苯、CS2及複閤溶劑 EOSA 萃取分離油砂瀝青的效果,確定 EOSA 為最佳萃取溶劑。研究瞭溫度、溶劑用量、時間對 EOSA 萃取分離油砂瀝青收率的影響。結果錶明,在萃取溫度30℃、劑砂比2 mL/ g 條件下萃取30 min,油砂瀝青的收率可達95%以上。再生實驗結果錶明,在60~80℃條件下,溶劑迴收率超過99%。該工藝具有無水參與、零排放、低能耗、高收率等優點。
이극랍마의유사위실험대상,고찰석유미、배기완、정무완、정경완、갑분、CS2급복합용제 EOSA 췌취분리유사력청적효과,학정 EOSA 위최가췌취용제。연구료온도、용제용량、시간대 EOSA 췌취분리유사력청수솔적영향。결과표명,재췌취온도30℃、제사비2 mL/ g 조건하췌취30 min,유사력청적수솔가체95%이상。재생실험결과표명,재60~80℃조건하,용제회수솔초과99%。해공예구유무수삼여、령배방、저능모、고수솔등우점。
Take Karamay oil sands as a experimental subject,investigate the extraction and separation re-sult of oil sands bitumen with various solvents including petroleum ether,cyclohexane,n-pentane,n-hep-tane,toluene,carbon disulfide and composite solvents EOSA. EOSA is selected as the optimal solvent. The effect of extraction temperature,amount of solvent and the extraction time to the yield of oil sands bitumen was investigated. The result shows that under the conditions of extraction temperature of 30 ℃ ,solvent to oil sands ratio of 2 mL/ g,extraction time of 30 min,the yield of oil sands bitumen can reach above 95% . The regeneration experimental result shows,under the conditions of 60 ~ 80 ℃,more than 99% of the sol-vent can be recyclable. This process has various advantages including anhydrius participation,zero emis-sions,low energy consumption,high yield and so on.