大连民族学院学报
大連民族學院學報
대련민족학원학보
JOURNAL OF DALIAN UNIVERSITY FOR NATIONAL MINORITIES
2012年
3期
213-216
,共4页
石浩明%张树彪%陈会英%赵轶男%崔韶晖%那立艳%华瑞年
石浩明%張樹彪%陳會英%趙軼男%崔韶暉%那立豔%華瑞年
석호명%장수표%진회영%조질남%최소휘%나립염%화서년
壳聚糖%四氧化三铁%静电自组装%复合纳米颗粒
殼聚糖%四氧化三鐵%靜電自組裝%複閤納米顆粒
각취당%사양화삼철%정전자조장%복합납미과립
chitosan%iron oxide%electrostatic assembly%nanocomplex
以柠檬酸为改性剂,制备水基Fe3O4磁性纳米粒子,基于静电自组装作用,使壳聚糖分子在水溶液中包覆Fe3O4纳米晶粒,获得壳聚糖/Fe3O4复合纳米颗粒液溶胶。扫描电子显微镜(SEM)分析结果表明,复合纳米颗粒平均粒径为49.0nm,标准差为11.0nm。X射线衍射(XRD)和红外光谱(FT-IR)分析结果表明,复合纳米颗粒由壳聚糖分子和Fe3O4晶体粒子构成。
以檸檬痠為改性劑,製備水基Fe3O4磁性納米粒子,基于靜電自組裝作用,使殼聚糖分子在水溶液中包覆Fe3O4納米晶粒,穫得殼聚糖/Fe3O4複閤納米顆粒液溶膠。掃描電子顯微鏡(SEM)分析結果錶明,複閤納米顆粒平均粒徑為49.0nm,標準差為11.0nm。X射線衍射(XRD)和紅外光譜(FT-IR)分析結果錶明,複閤納米顆粒由殼聚糖分子和Fe3O4晶體粒子構成。
이저몽산위개성제,제비수기Fe3O4자성납미입자,기우정전자조장작용,사각취당분자재수용액중포복Fe3O4납미정립,획득각취당/Fe3O4복합납미과립액용효。소묘전자현미경(SEM)분석결과표명,복합납미과립평균립경위49.0nm,표준차위11.0nm。X사선연사(XRD)화홍외광보(FT-IR)분석결과표명,복합납미과립유각취당분자화Fe3O4정체입자구성。
The magnetic fluid was prepared by modifying the surface of F% 04 nanoparticles with citric acid. These Fe3O4 nanoparticles encapsulated by chitosan molecules through electrostatic force could be readily dispersed in aqueous solution. It was found in the SEM image that the aver- age diameter of nanocomplex was 49.0 nm, standard deviation was 11.0 nmo The particles prepared from chitosan and Fe3O4 were characterized by XRD and FF- IR nanocomplex analysis.