广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
5期
203-204
,共2页
周魁%党璐%张存社%沈寒晰%张金峰%蓝伟
週魁%黨璐%張存社%瀋寒晰%張金峰%藍偉
주괴%당로%장존사%침한석%장금봉%람위
高效液相色谱%纽甜%甜味剂%精密度
高效液相色譜%紐甜%甜味劑%精密度
고효액상색보%뉴첨%첨미제%정밀도
HPLC%neotame%sweetener%RSD
纽甜是一种新型高效、非营养型甜味剂,作为食品添加剂广泛应用在食品工业。对于纽甜产品的测量,目前尚没有国家标准,文章建立了用高效液相色谱法测定纽甜的含量,流动相为乙腈—缓冲溶液(体积比为25∶75),流速1.5 mL/min,二极管阵列检测器(DAD),柱温45℃。结果表明,纽甜质量浓度在1~10 mg/mL范围内甜与峰面积呈良好的线性关系,回收率在95.96%~99.90%。该方法简单、灵敏、准确,适用于纽含量的检测。
紐甜是一種新型高效、非營養型甜味劑,作為食品添加劑廣汎應用在食品工業。對于紐甜產品的測量,目前尚沒有國傢標準,文章建立瞭用高效液相色譜法測定紐甜的含量,流動相為乙腈—緩遲溶液(體積比為25∶75),流速1.5 mL/min,二極管陣列檢測器(DAD),柱溫45℃。結果錶明,紐甜質量濃度在1~10 mg/mL範圍內甜與峰麵積呈良好的線性關繫,迴收率在95.96%~99.90%。該方法簡單、靈敏、準確,適用于紐含量的檢測。
뉴첨시일충신형고효、비영양형첨미제,작위식품첨가제엄범응용재식품공업。대우뉴첨산품적측량,목전상몰유국가표준,문장건립료용고효액상색보법측정뉴첨적함량,류동상위을정—완충용액(체적비위25∶75),류속1.5 mL/min,이겁관진렬검측기(DAD),주온45℃。결과표명,뉴첨질량농도재1~10 mg/mL범위내첨여봉면적정량호적선성관계,회수솔재95.96%~99.90%。해방법간단、령민、준학,괄용우뉴함량적검측。
Neotame is a new non-nutritive high-intensity sweetener,as a food additive widely used in food industry.There is currently no national standard for measurement of the neotame sweet products.The structure,performance and development trends of neotame are introduced.A high performance liquid chromatographic method was developed to determine of amounts of neotame in the paper.A mobile phase of acetonitrile-buffer solution(25∶75,V/V) at a flow rateof 1.5 mL/min and column temperature 45 ℃ with diode-array detector were adopeted.The method was proved tobe linear in the neotame from 1~10 mg/mL.The recovery was 95.96 %~99.90 %.The established method has been successfully applied to the determination of the amounts of neotame.