广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
5期
309-310,312
,共3页
三氟甲基苯胺%核磁共振%结构解析
三氟甲基苯胺%覈磁共振%結構解析
삼불갑기분알%핵자공진%결구해석
Trifluoromethyl benzenamine%NMR%structure analysis
通过1H-1H COSY、HSQC和HMBC等2D NMR技术对3-三氟甲基-4-[（4-甲基哌嗪-1-基）甲基]苯胺的1H NMR和13C NMR谱进行了全归属,给出了相应的耦合常数。
通過1H-1H COSY、HSQC和HMBC等2D NMR技術對3-三氟甲基-4-[（4-甲基哌嗪-1-基）甲基]苯胺的1H NMR和13C NMR譜進行瞭全歸屬,給齣瞭相應的耦閤常數。
통과1H-1H COSY、HSQC화HMBC등2D NMR기술대3-삼불갑기-4-[（4-갑기고진-1-기）갑기]분알적1H NMR화13C NMR보진행료전귀속,급출료상응적우합상수。
An intermediate compound which may have potential pharmaceutical applications,3-（trifluoromethyl）-4-[（4-methylpiperazin-1-yl）methyl]benzenamine,was synthesized in our laboratory.In this paper,the 1H and 13C NMR signals of this compound were assigned completely using 2D NMR techniques such as 1H-1H COSY,HSQC and HMBC techniques.The corresponding coupling constants of the compound were also given out.
