绝缘材料
絕緣材料
절연재료
INSULATING MATERIALS
2014年
1期
48-51
,共4页
环氧树脂固化剂%钛酸叔胺酯%浇铸胶
環氧樹脂固化劑%鈦痠叔胺酯%澆鑄膠
배양수지고화제%태산숙알지%요주효
epoxy resin curing agent%tertiary amine titanate%casting resin
以钛酸正丁酯和三异丙醇胺为原料,在一定工艺条件下制备了钛酸叔胺酯固化剂,然后与E-51环氧树脂复配制备了电气绝缘浇铸料,分析了制备钛酸叔胺酯的各种影响因素和浇铸胶的性能等。结果表明:制备钛酸叔胺酯的最佳工艺条件为:钛酸正丁酯与三异丙醇胺的摩尔比为3∶4,真空度2660~3990 Pa,反应温度120~130℃;配制的浇铸料力学性能和电气性能优异,可满足应用要求。
以鈦痠正丁酯和三異丙醇胺為原料,在一定工藝條件下製備瞭鈦痠叔胺酯固化劑,然後與E-51環氧樹脂複配製備瞭電氣絕緣澆鑄料,分析瞭製備鈦痠叔胺酯的各種影響因素和澆鑄膠的性能等。結果錶明:製備鈦痠叔胺酯的最佳工藝條件為:鈦痠正丁酯與三異丙醇胺的摩爾比為3∶4,真空度2660~3990 Pa,反應溫度120~130℃;配製的澆鑄料力學性能和電氣性能優異,可滿足應用要求。
이태산정정지화삼이병순알위원료,재일정공예조건하제비료태산숙알지고화제,연후여E-51배양수지복배제비료전기절연요주료,분석료제비태산숙알지적각충영향인소화요주효적성능등。결과표명:제비태산숙알지적최가공예조건위:태산정정지여삼이병순알적마이비위3∶4,진공도2660~3990 Pa,반응온도120~130℃;배제적요주료역학성능화전기성능우이,가만족응용요구。
A tertiary amine titanate was synthesized by copolymerization of tetrabutyl titanate and tri-iso-propanolamine under certain process condition. A casting plastic was prepared by mixing tertiary amine ti-tanate and E-51 epoxy resin, and different influence factors in the preparation of tertiary amine titanate and the properties of the casting plastic were studied. The results show that the optimum process condi-tion in preparation of tertiary amine titanate is that the molar ratio of tetrabutyl titanate and tri-isopropa-nolamine is 3∶4, the vacuum degree is 2 660~3 990 Pa, and the reaction temperature is 120~130℃. The prepared casting plastic has excellent mechanical and electrical properties, which can satisfy the applica-tion requirements.