CAJ | 학술논문

　　目的对酒石酸长春瑞滨中的残留溶剂进行测定。方法采用溶液直接进样气相色谱法，DB-5（30 m ×0.53 mm×1.0μm）石英毛细管色谱柱，氢火焰离子化检测器，载气为氮气；进样口温度为150℃，检测器温度为210℃，柱温为40℃。结果被测溶剂均能得到很好的分离，每一个溶剂的峰面积与浓度在一定线性范围内均呈良好的线性关系。结论该方法作为酒石酸长春瑞滨中残留溶剂的检测是准确的、可靠的。
　　목적대주석산장춘서빈중적잔류용제진행측정。방법채용용액직접진양기상색보법，DB-5（30 m ×0.53 mm×1.0μm）석영모세관색보주，경화염리자화검측기，재기위담기；진양구온도위150℃，검측기온도위210℃，주온위40℃。결과피측용제균능득도흔호적분리，매일개용제적봉면적여농도재일정선성범위내균정량호적선성관계。결론해방법작위주석산장춘서빈중잔류용제적검측시준학적、가고적。
Objective To establish the method for detection of residual solvents in vinorelbine tartrate. Methods The residual solvents in vinorelbine tartrate was determined by solution dired-injection GC with DB-5 capillary column (30 m×0.53 mm×1.0 μm) with FID detector and nitrogen as the carries gas. The injector temperature was 150 ℃ , the detector temperature was 210 ℃ , the column temperature was 40 ℃ . Results The solvents could be completely separated, and the calibration curves of each solvent had good linear relationship within a certain range. Conclusion The method is proved accurate and reliable. It can be used for the determination of residual solvents in vinorelbine tartrate.