广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
15期
157-158
,共2页
高效液相色谱法%丹黄祛瘀胶囊%丹参素钠
高效液相色譜法%丹黃祛瘀膠囊%丹參素鈉
고효액상색보법%단황거어효낭%단삼소납
HPLC%Danhuang Quyu capsule%sodium danshensu
建立了丹黄祛瘀胶囊中丹参素钠的含量测定方法。采用Agilent C18柱（250 mm×4.6 mm,5μm）,流动相为甲醇-0.1%磷酸（10∶95）,柱温30℃,流速1.0 mL/min,检测波长280 nm。结果表明：丹参素钠在0.279～3.069μg内线性关系良好（r=0.9995）;平均回收率为99.2%,RSD=0.87%（n=6）,该法可用于控制丹黄祛瘀胶囊的质量。
建立瞭丹黃祛瘀膠囊中丹參素鈉的含量測定方法。採用Agilent C18柱（250 mm×4.6 mm,5μm）,流動相為甲醇-0.1%燐痠（10∶95）,柱溫30℃,流速1.0 mL/min,檢測波長280 nm。結果錶明：丹參素鈉在0.279～3.069μg內線性關繫良好（r=0.9995）;平均迴收率為99.2%,RSD=0.87%（n=6）,該法可用于控製丹黃祛瘀膠囊的質量。
건립료단황거어효낭중단삼소납적함량측정방법。채용Agilent C18주（250 mm×4.6 mm,5μm）,류동상위갑순-0.1%린산（10∶95）,주온30℃,류속1.0 mL/min,검측파장280 nm。결과표명：단삼소납재0.279～3.069μg내선성관계량호（r=0.9995）;평균회수솔위99.2%,RSD=0.87%（n=6）,해법가용우공제단황거어효낭적질량。
To establish a HPLC method for determination of Sodium Danshensu in Danhuang Quyu capsule.An Agilent C18 column（4.6 nm×250 mm,5 μm） was used,the mobile phase was methanol-0.1% phosphoric acid（10：95）,the detection wavelength was 280 nm,the column temperatuer was 30 ℃ and the flow rate was 1.0 mL·min-1.Sodium Danshensu showed a good linear relationship in the range of was 0.279~3.069 μg（r=0.9995）,the average recovery was 99.2%,RSD=0.87%（n=6）.The method is accurate and reliable,it can be used for the quality control of Danhuang Quyu capsule.
