山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2012年
10期
3-4
,共2页
烃化%水解%脱羧
烴化%水解%脫羧
경화%수해%탈최
hydrocarbons%hydrolysis%decarboxylation
介绍了一种合成丙戊酸钠的新工艺,以价格便宜的丙二酸二甲酯为原料,经烃化、水解、脱羧、成盐合成丙戊酸钠,采用PEG-400为催化剂,缩短了反应时间,提高了反应收率,降低了生产成本,简化了反应工序,更又有利于工业化生产。
介紹瞭一種閤成丙戊痠鈉的新工藝,以價格便宜的丙二痠二甲酯為原料,經烴化、水解、脫羧、成鹽閤成丙戊痠鈉,採用PEG-400為催化劑,縮短瞭反應時間,提高瞭反應收率,降低瞭生產成本,簡化瞭反應工序,更又有利于工業化生產。
개소료일충합성병무산납적신공예,이개격편의적병이산이갑지위원료,경경화、수해、탈최、성염합성병무산납,채용PEG-400위최화제,축단료반응시간,제고료반응수솔,강저료생산성본,간화료반응공서,경우유리우공업화생산。
The introduction of the new technology of a synthetic sodium valproate Takeing dimethylmalonate as raw materials, synthesis of sodium valproate, by alkylation, hydrolysis, salfication. Reducing the production costs. The using of PEG - 400 as catalyst, shortened the reaction time and improved the reaction yield, simplified the reaction step, and the more there were industrially advantageous production.