中国兽药杂志
中國獸藥雜誌
중국수약잡지
CHINESE JOURNAL OF VETERINARY DRUG
2012年
11期
37-38
,共2页
李毅竦%唐建%刁培渊%杨武宁%覃雪斌%何琼
李毅竦%唐建%刁培淵%楊武寧%覃雪斌%何瓊
리의송%당건%조배연%양무저%담설빈%하경
大黄%山大黄%土大黄苷%鉴别
大黃%山大黃%土大黃苷%鑒彆
대황%산대황%토대황감%감별
Dahuang%Shandahuang%rhapontin%identification
选用企业报批的大黄末为供试品,对2010年版《中国兽药典》收载的大黄、山大黄单味制剂的鉴别和检查项目以及大黄复方制剂的检查项目进行了研究和分析,认为用纸层析、硅胶薄层鉴别的技术检查土大黄苷是制剂中大黄与山大黄鉴别的关键,建议在样品检验和标准制定时加以重视。
選用企業報批的大黃末為供試品,對2010年版《中國獸藥典》收載的大黃、山大黃單味製劑的鑒彆和檢查項目以及大黃複方製劑的檢查項目進行瞭研究和分析,認為用紙層析、硅膠薄層鑒彆的技術檢查土大黃苷是製劑中大黃與山大黃鑒彆的關鍵,建議在樣品檢驗和標準製定時加以重視。
선용기업보비적대황말위공시품,대2010년판《중국수약전》수재적대황、산대황단미제제적감별화검사항목이급대황복방제제적검사항목진행료연구화분석,인위용지층석、규효박층감별적기술검사토대황감시제제중대황여산대황감별적관건,건의재양품검험화표준제정시가이중시。
Choosing Dahuang powder from enterprises that submit for approval as the samples, the identification and inspection project of Dahuang and Shandahuang single herb preparations, and the inspection project of the Dahuang compound preparation, which were recorded in Veterinary Pharmacopoeia of PRC (2010 edition) , were studied and analyzed in this article. It claims that examining rhapontin by paper chromatography and silicon thin layer is the key factor in the identification of Dahuang and Shandahuang in preparation. It suggests that this method should be paid more attention in sample testing and standard setting progress.