CAJ | 학술논문

以丙酮与苯基三氯硅烷为原料、氯化亚铜为催化剂、三乙胺为缚酸剂、苯为溶剂，合成了苯基三异丙烯氧基硅烷。当反应温度为50°C时，产品收率在43％左右。通过红外、核磁共振氢谱和碳谱及裂解质谱对产物结构进行了表征；并将其作为交联剂，配成了脱丙酮型室温硫化硅橡胶，硫化后的硅橡胶具有较好的介电性能和机械性能。
이병동여분기삼록규완위원료、록화아동위최화제、삼을알위박산제、분위용제，합성료분기삼이병희양기규완。당반응온도위50°C시，산품수솔재43％좌우。통과홍외、핵자공진경보화탄보급렬해질보대산물결구진행료표정；병장기작위교련제，배성료탈병동형실온류화규상효，류화후적규상효구유교호적개전성능화궤계성능。
Phenyltriisopropenyloxysilane was synthesized with cuprous chloride as catalyzer , triethylamine as deacid reagent , acetone and phenylrichlorosilane as raw materials .The product yield was 43%when the re-action temperature was 50°C.Its microstructure was analyzed and characterized by FTIR , 1 H NMR, 13 C NMR and MS .The prepared phenyltriisopropenyloxysilane was used as the across-linking agent to prepare deaceton-ized room temperature vulcanization ( RTV-1) silicone rubber and the vulcanized silicone rubber showed good dielectric and mechanical properties .