CAJ | 학술논문

评定了电感偶合等离子体质谱法测定水中的铅含量的不确定度，系统地分析了影响其测定的不确定度的各种因素，建立了测量过程中各分量的数学模型。最终确定了测定结果的包含区间，得出影响铅含量测定不确定度的主要来源是仪器的回收率和标准溶液配制所引入的不确定度，在测定过程中应给予足够的重视。
평정료전감우합등리자체질보법측정수중적연함량적불학정도，계통지분석료영향기측정적불학정도적각충인소，건립료측량과정중각분량적수학모형。최종학정료측정결과적포함구간，득출영향연함량측정불학정도적주요래원시의기적회수솔화표준용액배제소인입적불학정도，재측정과정중응급여족구적중시。
The uncertainty of determination of lead in water by ICP-MSis was evaluated ,and all kinds of influence factors which impacted upon the uncertainty of the determination were analyzed ,then mathematical model of the components in measurement process was established.Ultimately ,it confirmed the interval of the determination results ,and reached the conclusion that the uncertainty introduced of recovery and standard solution preparation was the prime source of the determination of lead.It should be paid more attentions during the measurement.