CAJ | 학술논문

研究了用大孔径毛细管柱定量分析唑虫酰胺方法。色谱条件如下：DB-115m×0.53×0.5μm。柱温215℃,进样口和检测器温度250℃,载气N2 13mL/min。邻苯二甲酸二癸酯作内标物。本方法在0.625～7.5μg质量的进样范围内和峰面积呈线性。相关系数（R）0.999 8唑虫酰胺分析的回收率为99.95%。
연구료용대공경모세관주정량분석서충선알방법。색보조건여하：DB-115m×0.53×0.5μm。주온215℃,진양구화검측기온도250℃,재기N2 13mL/min。린분이갑산이계지작내표물。본방법재0.625～7.5μg질량적진양범위내화봉면적정선성。상관계수（R）0.999 8서충선알분석적회수솔위99.95%。
A method of quantitative analysis for tolfenpxrad by a wide bore capillary column has been studied. Conditions were as follows. Column： 15m ×0.53mm ×0.51μm DB-1; column temperature： 215℃; temperatures of injector and detector： 250℃, and carried gas： N2 13 mL/ min.. The 1, 2-Benzenedicarboxylicacid, 1, 2-didecyl ester was used as internal standard. This analytical method is linear and reproducible over the range 0.625 -7.5μg analyte. A fit these data to a straight line using a least- correlation coefficient yields an R value of 0.9998. The recoveries was 99.95%.