CAJ | 학술논문

利用超高效液相色谱-串联质谱技术，建立了检测土壤样品中烟嘧磺隆残留量的分析方法。土壤样品用水和乙腈的混合溶液振荡提取，用UPLC—MS／MS测定。烟嘧磺隆在土壤中的平均回收率为83．1～106．2％，RSD为3．2～8．6％。该分析方法最低定量浓度为1．0μg／kg。该方法具有灵敏度高、操作简单、有机溶剂用量少等特点，可用于土壤样品中烟嘧磺隆的检测。
이용초고효액상색보-천련질보기술，건립료검측토양양품중연밀광륭잔류량적분석방법。토양양품용수화을정적혼합용액진탕제취，용UPLC—MS／MS측정。연밀광륭재토양중적평균회수솔위83．1～106．2％，RSD위3．2～8．6％。해분석방법최저정량농도위1．0μg／kg。해방법구유령민도고、조작간단、유궤용제용량소등특점，가용우토양양품중연밀광륭적검측。
The analysis method of nicosulfuron in soil was established using UPLC-MS/MS. The soil sample were extracted by the mixture of water and acetonitrile then determined by UPLC-MS/ MS. The average recoveries rate and RSD of nicosulfuron in soil were 83.1~106.2% and 3.2~8.6% respectively. The LOQ of the analysis method was 1.0 less use of organic solvent so that reliable to analysis μg/kg. The method was sensitive, simple and nicosulfuron residues in soil.