CAJ | 학술논문

建立了葡萄酒中14种农药残留的气相色谱-质谱联用选择离子模式进行监测的检测方法,样品采用正己烷∶乙酸乙酯（1∶1）萃取,无需净化。该方法在0.01～10 mg/L范围内线性关系良好,相关系数大于0.998;在0.01～1.0 mg/L添加水平范围内,平均加标回收率在90.32～108.13之间;最低检出限（LOD）在0.01～0.10 mg/kg之间,定量检出限（LOQ）为0.001～0.05 mg/kg,相对标准偏差均小于10%。
건립료포도주중14충농약잔류적기상색보-질보련용선택리자모식진행감측적검측방법,양품채용정기완∶을산을지（1∶1）췌취,무수정화。해방법재0.01～10 mg/L범위내선성관계량호,상관계수대우0.998;재0.01～1.0 mg/L첨가수평범위내,평균가표회수솔재90.32～108.13지간;최저검출한（LOD）재0.01～0.10 mg/kg지간,정량검출한（LOQ）위0.001～0.05 mg/kg,상대표준편차균소우10%。
A method （GC-MS coupled with liquid-liquid extraction） for rapid determination of 14 kinds of pesticides residue in grape wine has been developed. Grape wine samples were extracted by n-hexane and ethyl acetate （1：1） without purification. The results suggested that such method displayed good linear relationships within 0.01 - 1Q mg/L and the relative coefficient was above 0.998, the average recoveries were in the range of 90.32-108.13 with RSD s〈10 % as the addition level was between 0.01 -1.0 mg/L, LOD ranged from 0.01 -0.10 mg/kg, and LOQ ranged from 0.001 -0.05 mg/kg.