CAJ | 학술논문

介绍了使用X射线荧光光谱法测定氧化铝陶瓷主次量成分。用熔融玻璃片法制样，此方法简单，迅速，成本低。选用铝土矿GBW07177～GBW07182和GSB04—2606—2010系列标准样品，采用仪器软件SuperQ中提供的飞利浦模式的经验系数（Classic）和基本参数法校正元素间的谱线重叠干扰和基体效应，使用Magix（PW2403）x射线荧光光谱仪对样品中的Al2O3，SiO2，Fe2O3，TiO2，K2O，Na2O，CaO和Mg0共8个元素进行测定，各组分的RSD均小于3．36％，测量结果与计算值的误差在化学分析允许差范围内。
개소료사용X사선형광광보법측정양화려도자주차량성분。용용융파리편법제양，차방법간단，신속，성본저。선용려토광GBW07177～GBW07182화GSB04—2606—2010계렬표준양품，채용의기연건SuperQ중제공적비리포모식적경험계수（Classic）화기본삼수법교정원소간적보선중첩간우화기체효응，사용Magix（PW2403）x사선형광광보의대양품중적Al2O3，SiO2，Fe2O3，TiO2，K2O，Na2O，CaO화Mg0공8개원소진행측정，각조분적RSD균소우3．36％，측량결과여계산치적오차재화학분석윤허차범위내。
A method has been developed for the determination of Al2O3 ,SiO2 ,Fe2O3 ,TiO2 , K2O ,Na2O, CaO and MgO in alumina ceramic by An X - ray fluorescence spectrometric Magix （ PW2403 ） with fused glass disk mdthod and GBW07177 -GBW07182 ,GSB 04 -2606 -2010 standard samples . The inter element and matrix effects were corrected by using empirical alpha（or） coefficient program（ Classic）provided by the SuperQ and basic parameters. The RSD＇s obtained were less than 3.5%. The discrepancies between the results obtained by the present method and the calculate values were within the allowable range of chemical analysis.