齐鲁石油化工
齊魯石油化工
제로석유화공
QILU PETROCHEMICAL TECHNOLOGY
2012年
2期
155-159
,共5页
韩新竹%周忠国%许金山%许晓斌%靳丽君
韓新竹%週忠國%許金山%許曉斌%靳麗君
한신죽%주충국%허금산%허효빈%근려군
微反活性指数%气相色谱%催化剂%催化裂化
微反活性指數%氣相色譜%催化劑%催化裂化
미반활성지수%기상색보%최화제%최화열화
microreating reactivity index%chromatography%catalyst%catalytic cracking
主要介绍了利用新型岛津GC-2014C氢火焰色谱仪测定催化裂化催化剂微反活性指数的方法研究。通过考察柱初温、终温、程序升温速率以及汽化室和检测器的温度等色谱条件,确定了标准样品中汽油含量的校正因子(K)值。测定结果表明,该方法具有重复性好、准确度及检测灵敏度高等优点。
主要介紹瞭利用新型島津GC-2014C氫火燄色譜儀測定催化裂化催化劑微反活性指數的方法研究。通過攷察柱初溫、終溫、程序升溫速率以及汽化室和檢測器的溫度等色譜條件,確定瞭標準樣品中汽油含量的校正因子(K)值。測定結果錶明,該方法具有重複性好、準確度及檢測靈敏度高等優點。
주요개소료이용신형도진GC-2014C경화염색보의측정최화열화최화제미반활성지수적방법연구。통과고찰주초온、종온、정서승온속솔이급기화실화검측기적온도등색보조건,학정료표준양품중기유함량적교정인자(K)치。측정결과표명,해방법구유중복성호、준학도급검측령민도고등우점。
The paper studied test method of microreating reactivity index of FCC catalyst by new type shimadzu GC -2014C hydrogen flame chromatograph. Start temperature, final temper- ature and temperature - programmed rate of the column, temperature of vaporizing chamber and detector were investigated, value of correction factor (K) for gasoline content in standard sam- ple was determined. The test results showed the method possessed many advantages, such as good repeatability, high accuracy and detection sensitively etc.