CAJ | 학술논문

建立了角鲨烯软胶囊中角鲨烯含量的毛细管气相色谱测定方法。该法采用WBI进样口，毛细管色谱柱SGEAC20（PEG20M，30m×0．53mm×1μm），FID检测器进行检测。进样口温度：250℃，载气流速：6mL／min，柱室温度：230℃恒温，检测器温度：250℃，样品用正己烷定容后直接进样测定。方法简单、快速、重现性好，平均回收率大于99％，RSD小于3．0％，线性范围为25mg／L--400mg／L。
건립료각사희연효낭중각사희함량적모세관기상색보측정방법。해법채용WBI진양구，모세관색보주SGEAC20（PEG20M，30m×0．53mm×1μm），FID검측기진행검측。진양구온도：250℃，재기류속：6mL／min，주실온도：230℃항온，검측기온도：250℃，양품용정기완정용후직접진양측정。방법간단、쾌속、중현성호，평균회수솔대우99％，RSD소우3．0％，선성범위위25mg／L--400mg／L。
A method is established for the determination of Squalene in Squalene Soft Capsules by Capillary GC. The separation was achieved by using WBI injection port, Capillary GC column SGE AC20（30m × 0.53 mm ×μ m）, FID detector. Injecton temperature： 250℃, flow of cartier gas： 6 mL/min , column oven temperature： 230℃, detector temperature： 250℃. the method is accurate, rapid and convenient, the results indicate that the recovery is more than 99%, RSD is less than 3.0% and the working curves of Squalene was in the linear range 25mg/L-400mg/L.